2-N-acetyl-3,4,6-tri-O-benzyl-1,2-dideoxy-1,2-di-(p-toluenesulfonamido)-β-D-glucopyranose

Base Information

• Chemical Name: 2-N-acetyl-3,4,6-tri-O-benzyl-1,2-dideoxy-1,2-di-(p-toluenesulfonamido)-β-D-glucopyranose
• CAS No.: 1001200-75-4
• Molecular Formula: C₄₃H₄₆N₂O₉S₂
• Molecular Weight: 798.978

Synonyms:2-N-acetyl-3,4,6-tri-O-benzyl-1,2-dideoxy-1,2-di-(p-toluenesulfonamido)-β-D-glucopyranose

Chemical Property of 2-N-acetyl-3,4,6-tri-O-benzyl-1,2-dideoxy-1,2-di-(p-toluenesulfonamido)-β-D-glucopyranose

Chemical Property:

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Technology Process of 2-N-acetyl-3,4,6-tri-O-benzyl-1,2-dideoxy-1,2-di-(p-toluenesulfonamido)-β-D-glucopyranose

There total 1 articles about 2-N-acetyl-3,4,6-tri-O-benzyl-1,2-dideoxy-1,2-di-(p-toluenesulfonamido)-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

3,4,6-tri-O-benzyl-1,2-dideoxy-1,2-di-(p-toluenesulfonamido)-β-D-glucopyranose (920968-69-0) + acetic anhydride (108-24-7) → 2-N-acetyl-3,4,6-tri-O-benzyl-1,2-dideoxy-1,2-di-(p-toluenesulfonamido)-β-D-glucopyranose (1001200-75-4)

Guidance literature:

With pyridine; dmap; at 20 ℃; for 24h;

DOI:10.1039/b712841j

Reference yield: 77.0%

2-N-acetyl-3,4,6-tri-O-benzyl-1,2-dideoxy-1,2-di-(p-toluenesulfonamido)-β-D-glucopyranose (1001200-75-4) → 2-acetamido-3,4,6-tri-O-benzyl-1,2-dideoxy-1-(p-toluenesulfonamido)-β-D-glucopyranose (1001200-78-7)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; In tetrahydrofuran; at 20 ℃; for 0.5h;

DOI:10.1039/b712841j

Reference yield:

2-N-acetyl-3,4,6-tri-O-benzyl-1,2-dideoxy-1,2-di-(p-toluenesulfonamido)-β-D-glucopyranose (1001200-75-4) + chloroformic acid ethyl ester (541-41-3) → C46H50N2O11S2 (1001200-80-1)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 6h;

DOI:10.1039/b712841j

upstream raw materials:

3,4,6-tri-O-benzyl-1,2-dideoxy-1,2-di-(p-toluenesulfonamido)-β-D-glucopyranose

acetic anhydride

Downstream raw materials:

2-acetamido-3,4,6-tri-O-benzyl-1,2-dideoxy-1-(p-toluenesulfonamido)-β-D-glucopyranose

C₄₆H₅₀N₂O₁₁S₂

C₄₇H₅₀N₂O₁₁S₂

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