C₃₁H₄₂ClNO₃Si

Base Information

Chemical Name:C₃₁H₄₂ClNO₃Si
CAS No.:87306-95-4
Molecular Formula:C₃₁H₄₂ClNO₃Si
Molecular Weight:540.218
Hs Code.:

C<sub>31</sub>H<sub>42</sub>ClNO<sub>3</sub>Si

Synonyms:C₃₁H₄₂ClNO₃Si

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Chemical Property of C₃₁H₄₂ClNO₃Si

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Technology Process of C₃₁H₄₂ClNO₃Si

There total 9 articles about C₃₁H₄₂ClNO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87306-91-0
[(1S,2S)-2-(tert-Butyl-dimethyl-silanyloxy)-1-methoxymethyl-2-phenyl-ethyl]-(6-methoxy-2'-methyl-biphenyl-2-ylmethyl)-amine

: 87306-95-4
C₃₁H₄₂ClNO₃Si

Guidance literature:: With N-chloro-succinimide; In dichloromethane; for 0.25h;
DOI:10.1021/ja00289a023

Reference yield:

: 1521-38-6
2,3-dimethoxybenzoic acid

: 87306-95-4
C₃₁H₄₂ClNO₃Si

Guidance literature:: Multi-step reaction with 7 steps

1: oxalyl chloride / CH₂Cl₂ / 14 h

2: 30 percent NH₄OH

3: 1.) triethyloxonium tetrafluoroborate / 1.) 1,2-dichloroethane, 22 h; 2.) 1,2-dichloroethane, 24 h, reflux

4: 1.) Mg / 1.) ether, 1 h; 2.) ether, THF, 24 h

5: 1 M DIBAL / diethyl ether / Ambient temperature

6: tetrahydrofuran / 12 h / Ambient temperature

7: N-chlorosuccinimide / CH₂Cl₂ / 0.25 h

With ammonium hydroxide; N-chloro-succinimide; oxalyl dichloride; triethyloxonium fluoroborate; diisobutylaluminium hydride; magnesium; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ja00289a023

Reference yield:

: 1521-39-7
2,3-dimethoxybenzamide

: 87306-95-4
C₃₁H₄₂ClNO₃Si

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) triethyloxonium tetrafluoroborate / 1.) 1,2-dichloroethane, 22 h; 2.) 1,2-dichloroethane, 24 h, reflux

2: 1.) Mg / 1.) ether, 1 h; 2.) ether, THF, 24 h

3: 1 M DIBAL / diethyl ether / Ambient temperature

4: tetrahydrofuran / 12 h / Ambient temperature

5: N-chlorosuccinimide / CH₂Cl₂ / 0.25 h

With N-chloro-succinimide; triethyloxonium fluoroborate; diisobutylaluminium hydride; magnesium; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ja00289a023