α-(difluoromethyl)-2-furanmethanol

Base Information

Chemical Name:α-(difluoromethyl)-2-furanmethanol
CAS No.:122590-90-3
Molecular Formula:C₁₂H₁₀F₂O₄S
Molecular Weight:288.272
Hs Code.:

α-(difluoro<phenylsulfonyl>methyl)-2-furanmethanol

Synonyms:α-(difluoromethyl)-2-furanmethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-(difluoromethyl)-2-furanmethanol

Chemical Property:

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Technology Process of α-(difluoromethyl)-2-furanmethanol

There total 10 articles about α-(difluoromethyl)-2-furanmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 98-01-1
furfural

: 1535-65-5
difluoromethyl phenyl sulfone

: 98-00-0,25212-86-6,93793-62-5
(2-furyl)methyl alcohol

: 122590-90-3
α-(difluoromethyl)-2-furanmethanol

Guidance literature:: With sodium hydroxide; Aliquat 336; In dichloromethane;
DOI:10.1016/S0022-1139(00)81636-X

Reference yield: 69.0%

: 98-01-1
furfural

: potassium 2-(phenylsulfonyl)-2,2-difluoroacetate

: 122590-90-3
α-(difluoromethyl)-2-furanmethanol

Guidance literature:: In N,N-dimethyl-formamide; at 28 ℃; for 15h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tetlet.2018.07.021

Reference yield: 56.0%

: 98-01-1
furfural

: 1535-65-5
difluoromethyl phenyl sulfone

: 122590-90-3
α-(difluoromethyl)-2-furanmethanol

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃; for 4h;
DOI:10.1016/j.jfluchem.2007.03.004