2-n-butyl-4-<(2'-carbamoylbiphenyl-4-yl)methyl>-5-phenyl-3H-imidazo<1,2-b><1,2,4>triazole

Base Information

Chemical Name:2-n-butyl-4-<(2'-carbamoylbiphenyl-4-yl)methyl>-5-phenyl-3H-imidazo<1,2-b><1,2,4>triazole
CAS No.:144936-14-1
Molecular Formula:C₂₈H₂₇N₅O
Molecular Weight:449.555
Hs Code.:

Synonyms:2-n-butyl-4-<(2'-carbamoylbiphenyl-4-yl)methyl>-5-phenyl-3H-imidazo<1,2-b><1,2,4>triazole

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Chemical Property of 2-n-butyl-4-<(2'-carbamoylbiphenyl-4-yl)methyl>-5-phenyl-3H-imidazo<1,2-b><1,2,4>triazole

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Technology Process of 2-n-butyl-4-<(2'-carbamoylbiphenyl-4-yl)methyl>-5-phenyl-3H-imidazo<1,2-b><1,2,4>triazole

There total 8 articles about 2-n-butyl-4-<(2'-carbamoylbiphenyl-4-yl)methyl>-5-phenyl-3H-imidazo<1,2-b><1,2,4>triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-amino-3-n-butyl-4-<(2'-cyanobiphenyl-4-yl)methyl>-1-phenacyl-4H-1,2,4-triazolium bromide

: 144936-15-2
2-n-butyl-4-<(2'-cyanobiphenyl-4-yl)methyl>-5-phenyl-3H-imidazo<1,2-b><1,2,4>triazole

: 144936-14-1
2-n-butyl-4-<(2'-carbamoylbiphenyl-4-yl)methyl>-5-phenyl-3H-imidazo<1,2-b><1,2,4>triazole

Guidance literature:: With poly(phosphoric acid); at 85 ℃; for 6h;
DOI:10.1021/jm00057a009

Reference yield:

: 114772-54-2
4'-(bromomethyl)-1,1'-biphenyl-2-carbonitrile

: 144936-14-1
2-n-butyl-4-<(2'-carbamoylbiphenyl-4-yl)methyl>-5-phenyl-3H-imidazo<1,2-b><1,2,4>triazole

Guidance literature:: Multi-step reaction with 6 steps

1: 68 percent / lithium azide / dimethylsulfoxide / 1 h / Ambient temperature

2: 89 percent / triphenylphosphine / 2 h / Ambient temperature

3: 71 percent / ethanol / 144 h / Ambient temperature

4: 64 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 5 h

5: 86 percent / ethanol / 8 h / 80 °C

6: 211 mg / poly(phosphoric acid) / 6 h / 85 °C

With lithium azide; poly(phosphoric acid); 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jm00057a009

Reference yield:

: 144936-09-4
ethyl valerate thiosemicarbazone

: 144936-14-1
2-n-butyl-4-<(2'-carbamoylbiphenyl-4-yl)methyl>-5-phenyl-3H-imidazo<1,2-b><1,2,4>triazole

Guidance literature:: Multi-step reaction with 5 steps

1: 41 percent / CH₂Cl₂ / 2.5 h / Ambient temperature

2: 71 percent / ethanol / 144 h / Ambient temperature

3: 64 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 5 h

4: 86 percent / ethanol / 8 h / 80 °C

5: 211 mg / poly(phosphoric acid) / 6 h / 85 °C

With poly(phosphoric acid); 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane;
DOI:10.1021/jm00057a009