(3S,6R,1'R,2'S,3'R)-3-[1'-benzyloxy-3'-methanesulfonyloxy-2',4'-ethylidenedioxybutyl]-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine

Base Information

Chemical Name:(3S,6R,1'R,2'S,3'R)-3-[1'-benzyloxy-3'-methanesulfonyloxy-2',4'-ethylidenedioxybutyl]-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine
CAS No.:1097198-51-0
Molecular Formula:C₂₃H₃₄N₂O₈S
Molecular Weight:498.598
Hs Code.:

Synonyms:(3S,6R,1'R,2'S,3'R)-3-[1'-benzyloxy-3'-methanesulfonyloxy-2',4'-ethylidenedioxybutyl]-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine

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Chemical Property of (3S,6R,1'R,2'S,3'R)-3-[1'-benzyloxy-3'-methanesulfonyloxy-2',4'-ethylidenedioxybutyl]-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine

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Technology Process of (3S,6R,1'R,2'S,3'R)-3-[1'-benzyloxy-3'-methanesulfonyloxy-2',4'-ethylidenedioxybutyl]-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine

There total 1 articles about (3S,6R,1'R,2'S,3'R)-3-[1'-benzyloxy-3'-methanesulfonyloxy-2',4'-ethylidenedioxybutyl]-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1097198-48-5
(3S,6R,1'R,2'S,3'R)-3-[1'-hydroxy-3'-methanesulfonyloxy-2',4'-ethylidenedioxybutyl]-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine

: 100-39-0
benzyl bromide

: 1097198-51-0
(3S,6R,1'R,2'S,3'R)-3-[1'-benzyloxy-3'-methanesulfonyloxy-2',4'-ethylidenedioxybutyl]-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine

Guidance literature:: (3S,6R,1'R,2'S,3'R)-3-[1'-hydroxy-3'-methanesulfonyloxy-2',4'-ethylidenedioxybutyl]-3,6-dihydro-6-isopropyl-2,5-dimethoxypyrazine; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 1h;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1039/b810878a