trans-N,N-dibenzyl-4-(2-(tetrahydro-2H-pyran-2-yloxy)ethoxy)cyclohexanamine

Base Information

Chemical Name:trans-N,N-dibenzyl-4-(2-(tetrahydro-2H-pyran-2-yloxy)ethoxy)cyclohexanamine
CAS No.:1359966-03-2
Molecular Formula:C₂₇H₃₇NO₃
Molecular Weight:423.596
Hs Code.:

Synonyms:trans-N,N-dibenzyl-4-(2-(tetrahydro-2H-pyran-2-yloxy)ethoxy)cyclohexanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-N,N-dibenzyl-4-(2-(tetrahydro-2H-pyran-2-yloxy)ethoxy)cyclohexanamine

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Technology Process of trans-N,N-dibenzyl-4-(2-(tetrahydro-2H-pyran-2-yloxy)ethoxy)cyclohexanamine

There total 3 articles about trans-N,N-dibenzyl-4-(2-(tetrahydro-2H-pyran-2-yloxy)ethoxy)cyclohexanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 17739-45-6,59146-56-4
2-(2-bromoethoxy)tetrahydropyran

: 32503-27-8
tetra(n-butyl)ammonium hydrogensulfate

: 149506-81-0
trans-4-(dibenzylamino)cyclohexanol

: 1359966-03-2
trans-N,N-dibenzyl-4-(2-(tetrahydro-2H-pyran-2-yloxy)ethoxy)cyclohexanamine

Guidance literature:: With SiO₂; In Petroleum ether;

Reference yield: 61.0%

: 17739-45-6,59146-56-4
2-(2-bromoethoxy)tetrahydropyran

: 149506-81-0
trans-4-(dibenzylamino)cyclohexanol

: 1359966-03-2
trans-N,N-dibenzyl-4-(2-(tetrahydro-2H-pyran-2-yloxy)ethoxy)cyclohexanamine

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 90 ℃; for 16h;

Reference yield:

: 27489-62-9
trans-4-hydroxycyclohexylamine

: 100-39-0
benzyl bromide

: 1359966-03-2
trans-N,N-dibenzyl-4-(2-(tetrahydro-2H-pyran-2-yloxy)ethoxy)cyclohexanamine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 16 h / 90 °C

2: sodium hydride / N,N-dimethyl-formamide / 16 h / 90 °C

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; acetonitrile;