hept-3-yl phenyl ketone

Base Information

• Chemical Name: hept-3-yl phenyl ketone
• CAS No.: 17180-41-5
• Molecular Formula: C₁₄H₂₀O
• Molecular Weight: 204.312
• Mol file: 17180-41-5.mol

Synonyms:hept-3-yl phenyl ketone

Chemical Property of hept-3-yl phenyl ketone

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of hept-3-yl phenyl ketone

There total 6 articles about hept-3-yl phenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

bromobenzene (108-86-1,52753-63-6) + d,l-2-ethylhexanal (123-05-7) → hept-3-yl phenyl ketone (17180-41-5)

Guidance literature:

With palladium diacetate; 9,10-phenanthrenequinone; potassium hydrogencarbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In acetone; at 20 ℃; for 24h; Reagent/catalyst; Irradiation;

DOI:10.1021/acscatal.0c02105

Reference yield: 57.0%

d,l-2-ethylhexanal (123-05-7) + Benzoylformic acid (611-73-4) → hept-3-yl phenyl ketone (17180-41-5)

Guidance literature:

With dipotassium peroxodisulfate; iron(III)-acetylacetonate; di-tert-butyl peroxide; In ethyl acetate; at 120 ℃; for 2h; Sealed tube;

DOI:10.1002/chem.202000114

Reference yield: 51.0%

phenylzinc chloride lithium chloride + S-ethyl 2-ethylhexanoic acid thioester → hept-3-yl phenyl ketone (17180-41-5)

Guidance literature:

With Ni(xantphos)(o-tolyl)Cl; In tetrahydrofuran; at 20 ℃; for 1.5h; Inert atmosphere; Schlenk technique;

DOI:10.1002/chem.201801887

upstream raw materials:

2-ethylhexanoic acid chloride

benzene

carbon disulfide

aluminium trichloride

Downstream raw materials:

(2-ethylhexyl)benzene