phenyl 2,3-di-O-benzyl-4-O-(2-naphthyl)methyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 2,3-di-O-benzyl-4-O-(2-naphthyl)methyl-1-thio-β-D-glucopyranoside
CAS No.:1456718-89-0
Molecular Formula:C₃₇H₃₆O₅S
Molecular Weight:592.756
Hs Code.:

Synonyms:phenyl 2,3-di-O-benzyl-4-O-(2-naphthyl)methyl-1-thio-β-D-glucopyranoside

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Chemical Property of phenyl 2,3-di-O-benzyl-4-O-(2-naphthyl)methyl-1-thio-β-D-glucopyranoside

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Technology Process of phenyl 2,3-di-O-benzyl-4-O-(2-naphthyl)methyl-1-thio-β-D-glucopyranoside

There total 9 articles about phenyl 2,3-di-O-benzyl-4-O-(2-naphthyl)methyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1456718-88-9
C₃₇H₃₄O₅S

: 1456718-89-0
phenyl 2,3-di-O-benzyl-4-O-(2-naphthyl)methyl-1-thio-β-D-glucopyranoside

Guidance literature:: With aluminum (III) chloride; lithium aluminium tetrahydride; In diethyl ether; dichloromethane; at 0 - 20 ℃;
DOI:10.1002/ejoc.201300681

Reference yield: 49.0%

: phenyl 2,3-di-O-benzyl-4-O-(2-naphthyl)methyl-1-thio-β-D-xylo-hex-5-enopyranoside

: 1456718-89-0
phenyl 2,3-di-O-benzyl-4-O-(2-naphthyl)methyl-1-thio-β-D-glucopyranoside

: phenyl 2,3-di-O-benzyl-4-O-(2-naphthyl)methyl-1-thio-α-L-idopyranoside

Guidance literature:: phenyl 2,3-di-O-benzyl-4-O-(2-naphthyl)methyl-1-thio-β-D-xylo-hex-5-enopyranoside; With borane-THF; In tetrahydrofuran; at 0 ℃; for 1.5h;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 0.833333h;
DOI:10.1002/ejoc.201800425

Reference yield:

: 100-39-0
benzyl bromide

: 1456718-89-0
phenyl 2,3-di-O-benzyl-4-O-(2-naphthyl)methyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 12 h / 0 - 20 °C

1.2: 0.25 h

2.1: lithium aluminium tetrahydride; aluminum (III) chloride / dichloromethane; diethyl ether / 0 - 20 °C

With aluminum (III) chloride; lithium aluminium tetrahydride; sodium hydride; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201300681