(±)-(2S,5R)-2,5-diallyl-N-(4-methoxyphenyl)pyrrolidine-1-sulfonamide

Base Information

Chemical Name:(±)-(2S*,5R*)-2,5-diallyl-N-(4-methoxyphenyl)pyrrolidine-1-sulfonamide
CAS No.:1613330-74-7
Molecular Formula:C₁₇H₂₄N₂O₃S
Molecular Weight:336.455
Hs Code.:

Synonyms:(±)-(2S*,5R*)-2,5-diallyl-N-(4-methoxyphenyl)pyrrolidine-1-sulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (±)-(2S*,5R*)-2,5-diallyl-N-(4-methoxyphenyl)pyrrolidine-1-sulfonamide

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Technology Process of (±)-(2S*,5R*)-2,5-diallyl-N-(4-methoxyphenyl)pyrrolidine-1-sulfonamide

There total 3 articles about (±)-(2S*,5R*)-2,5-diallyl-N-(4-methoxyphenyl)pyrrolidine-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 180585-93-7
trans-2,5-diallylpyrrolidine

: 848937-70-2
N-(4-methoxyphenyl)-2-oxooxazolidine-3-sulfonamide

: 1613330-74-7
(±)-(2S*,5R*)-2,5-diallyl-N-(4-methoxyphenyl)pyrrolidine-1-sulfonamide

Guidance literature:: N-(4-methoxyphenyl)-2-oxooxazolidine-3-sulfonamide; With dmap; triethylamine; In acetonitrile; at 75 ℃; for 1h; Inert atmosphere;

trans-2,5-diallylpyrrolidine; In acetonitrile; at 75 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tet.2019.04.031

Reference yield:

: C₁₁H₁₇NO₂*C₂HF₃O₂

: 848937-70-2
N-(4-methoxyphenyl)-2-oxooxazolidine-3-sulfonamide

: 1613330-74-7
(±)-(2S*,5R*)-2,5-diallyl-N-(4-methoxyphenyl)pyrrolidine-1-sulfonamide

Guidance literature:: With dmap; triethylamine; In acetonitrile; at 75 ℃; for 0.16h; Inert atmosphere;
DOI:10.1021/ol5015976

Reference yield:

: (±)-(E,2R*,5S*)-tert-butyl 2-allyl-5-[3-(trimethylsilyl)allyl]pyrrolidine-1-carboxylate

: 1613330-74-7
(±)-(2S*,5R*)-2,5-diallyl-N-(4-methoxyphenyl)pyrrolidine-1-sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / Inert atmosphere; Reflux

2: dmap; triethylamine / acetonitrile / 0.16 h / 75 °C / Inert atmosphere

With dmap; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/ol5015976