(E)-N-benzyl(methyl)-(2-propenylphenyl)amine

Base Information

• Chemical Name: (E)-N-benzyl(methyl)-(2-propenylphenyl)amine
• CAS No.: 1016170-35-6
• Molecular Formula: C₁₇H₁₉N
• Molecular Weight: 237.345
• Mol file: 1016170-35-6.mol

Synonyms:(E)-N-benzyl(methyl)-(2-propenylphenyl)amine

Chemical Property of (E)-N-benzyl(methyl)-(2-propenylphenyl)amine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (E)-N-benzyl(methyl)-(2-propenylphenyl)amine

There total 1 articles about (E)-N-benzyl(methyl)-(2-propenylphenyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

benzyl[2-(propen-1-yl)phenyl]amine (909726-02-9) + methyl iodide (74-88-4) → (E)-N-benzyl(methyl)-(2-propenylphenyl)amine (1016170-35-6)

Guidance literature:

benzyl[2-(propen-1-yl)phenyl]amine; With phenyllithium; In n-heptane; dibutyl ether; at 20 ℃; for 0.25h;

methyl iodide; In n-heptane; dibutyl ether; at 20 ℃; for 1h; Further stages.;

DOI:10.1021/jo702290f

Reference yield:

n-butyllithium (109-72-8,29786-93-4) + (E)-N-benzyl(methyl)-(2-propenylphenyl)amine (1016170-35-6) → benzyl(methyl)-[2-(2-methylhexyl)phenyl]amine + benzyl(methyl)-[2-(2-methylhexyl)phenyl]amine (1016170-36-7)

Guidance literature:

n-butyllithium; (E)-N-benzyl(methyl)-(2-propenylphenyl)amine; With (-)-sparteine; In hexane; at -15 ℃; for 4h;

With methanol; In hexane; Further stages. Title compound not separated from byproducts.;

DOI:10.1021/jo702290f

upstream raw materials:

benzyl[2-(propen-1-yl)phenyl]amine

methyl iodide

Downstream raw materials:

benzyl(methyl)-[2-(2-methylhexyl)phenyl]amine