tert-butyldimethyl 2-(4-(tert-butyldimethylsilyloxy)-3-methoxyphenyl)acetate

Base Information

Chemical Name:tert-butyldimethyl 2-(4-(tert-butyldimethylsilyloxy)-3-methoxyphenyl)acetate
CAS No.:78324-15-9
Molecular Formula:C₂₁H₃₈O₄Si₂
Molecular Weight:410.701
Hs Code.:

Synonyms:tert-butyldimethyl 2-(4-(tert-butyldimethylsilyloxy)-3-methoxyphenyl)acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyldimethyl 2-(4-(tert-butyldimethylsilyloxy)-3-methoxyphenyl)acetate

Chemical Property:

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Technology Process of tert-butyldimethyl 2-(4-(tert-butyldimethylsilyloxy)-3-methoxyphenyl)acetate

There total 2 articles about tert-butyldimethyl 2-(4-(tert-butyldimethylsilyloxy)-3-methoxyphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 306-08-1
Homovanillic acid

: 18162-48-6
tert-butyldimethylsilyl chloride

: 78324-15-9
tert-butyldimethyl 2-(4-(tert-butyldimethylsilyloxy)-3-methoxyphenyl)acetate

Guidance literature:: With 1H-imidazole; In tetrahydrofuran; at 20 ℃; for 14h; Inert atmosphere;
DOI:10.1002/anie.201305645

Reference yield:

: 78324-15-9
tert-butyldimethyl 2-(4-(tert-butyldimethylsilyloxy)-3-methoxyphenyl)acetate

Guidance literature:

Reference yield:

: 78324-15-9
tert-butyldimethyl 2-(4-(tert-butyldimethylsilyloxy)-3-methoxyphenyl)acetate

: 57444-62-9
resiniferatoxin

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / tetrahydrofuran; water / 1 h / 0 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 5.67 h / 20 °C

2.2: 0.58 h / 0 °C

With caesium carbonate; acetic acid; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/jacs.7b10177