3-Methyl-4-dimethylaminoazobenzene

Base Information

Chemical Name:3-Methyl-4-dimethylaminoazobenzene
CAS No.:3732-90-9
Molecular Formula:C₁₅H₁₇N₃
Molecular Weight:239.32
Hs Code.:2927000090
UNII:659HNU0ZCT
DSSTox Substance ID:DTXSID501038285
Nikkaji Number:J2.194F
Mol file:3732-90-9.mol

Synonyms:3-Methyl-4-dimethylaminoazobenzene;3-Methyl-4-DAB;3732-90-9;BRN 1842369;o-Toluidine, N,N-dimethyl-4-(phenylazo)-;3-Methyl-4-dimethyl aminoazobenzene;Benzenamine, N,N,2-trimethyl-4-(phenylazo)-;659HNU0ZCT;Benzenamine, N,N,2-trimethyl-4-(2-phenyldiazenyl)-;UNII-659HNU0ZCT;SCHEMBL3341207;DTXSID501038285;LS-154361;N,N-DIMETHYL-4-AMINO-3-METHYLAZOBENZENE;Benzenamine, N,N,2-trimethyl-4-(phenylazo)- (9CI);N,N,2-TRIMETHYL-4-(2-PHENYLDIAZENYL)BENZENAMINE

Suppliers and Price of 3-Methyl-4-dimethylaminoazobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 3-Methyl-4-dimethylaminoazobenzene

Chemical Property:

Vapor Pressure:3.24E-06mmHg at 25°C
Melting Point:120oC
Refractive Index:1.5610 (estimate)
Boiling Point:387.7°Cat760mmHg
Flash Point:188.3°C
PSA：27.96000
Density:1.01g/cm³
LogP:4.47640
XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:239.142247555
Heavy Atom Count:18
Complexity:269

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=CC(=C1)N=NC2=CC=CC=C2)N(C)C

Technology Process of 3-Methyl-4-dimethylaminoazobenzene

There total 4 articles about 3-Methyl-4-dimethylaminoazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77-78-1
dimethyl sulfate

: 64-01-7
2,N-dimethyl-4-phenylazo-aniline

: 3732-90-9
2,N,N-trimethyl-4-phenylazo-aniline

Guidance literature:: With benzene;
DOI:10.1084/jem.87.2.139

Reference yield:

: 3732-90-9
2,N,N-trimethyl-4-phenylazo-aniline

Guidance literature:

Reference yield:

: 609-72-3
N,N-dimethyl-o-toluidine

: 3732-90-9
trans-3-Methyl-4-dimethylamino-azobenzol

Guidance literature:: Multi-step reaction with 3 steps

1: (i) aq. HCl, (ii) aq. NaNO₂, (iii) /BRN= 2205144/, aq. HCl

2: Al, aq. HCl

3: AcOH

With hydrogenchloride; acetic acid; aluminium;