diethyl N-<4-amino>ethyl>-N-methylamino>benzoyl>-L-glutamate

Base Information

Chemical Name:diethyl N-<4-amino>ethyl>-N-methylamino>benzoyl>-L-glutamate
CAS No.:107716-38-1
Molecular Formula:C₄₀H₅₁Cl₆N₈O₁₅P
Molecular Weight:1127.58
Hs Code.:

diethyl N-<4-<N-<2-<N-(2-amino-4-oxo-6-methylpyrimidin-5-yl)-N-<(3'-O-acetyl-2'-deoxyuridin-5-yl)methyl>amino>ethyl>-N-methylamino>benzoyl>-L-glutamate

Synonyms:diethyl N-<4-amino>ethyl>-N-methylamino>benzoyl>-L-glutamate

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Chemical Property of diethyl N-<4-amino>ethyl>-N-methylamino>benzoyl>-L-glutamate

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Technology Process of diethyl N-<4-amino>ethyl>-N-methylamino>benzoyl>-L-glutamate

There total 7 articles about diethyl N-<4-amino>ethyl>-N-methylamino>benzoyl>-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 88543-89-9
Acetic acid (2R,3S,5R)-2-[bis-(2,2,2-trichloro-ethoxy)-phosphoryloxymethyl]-5-(5-bromomethyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

: 107716-34-7
diethyl N-<4-ethyl>-N-methylamino>benzoyl>-L-glutamate

: 107716-38-1
diethyl N-<4-amino>ethyl>-N-methylamino>benzoyl>-L-glutamate

Guidance literature:: With sodium hydrogencarbonate; In N,N-dimethyl-formamide; for 2h; Ambient temperature;
DOI:10.1021/jm00119a012

Reference yield:

: 13726-52-8
diethyl N-(p-aminobenzoyl)-L-glutamate

: 107716-38-1
diethyl N-<4-amino>ethyl>-N-methylamino>benzoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 7 steps

1: 94 percent / sodium cyanoborohydride, bromocresol green, acetic acid / ethanol / 48 h / Ambient temperature

2: 91 percent / sodium cyanoborohydride, bromocresol green, aq. acetic acid / acetonitrile / 1 h / Ambient temperature

3: 80 percent / hydrogen, HCl / palladium on carbon / ethanol / 3 h / 2482.3 Torr

4: aq. acetic acid / 1.) 0 deg C, 2.) room temperature, 17 h

5: 80 percent / pyridine / 1 h / Ambient temperature

6: 20 percent / dimethylformamide / 24 h / 90 - 100 °C

7: 42 percent / NaHCO₃ / dimethylformamide / 2 h / Ambient temperature

With hydrogenchloride; hydrogen; bromocresol green; sodium cyanoborohydride; sodium hydrogencarbonate; acetic acid; palladium on activated charcoal; In pyridine; ethanol; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm00119a012

Reference yield:

: 115827-03-7
diethyl N--L-glutamate

: 107716-38-1
diethyl N-<4-amino>ethyl>-N-methylamino>benzoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / hydrogen, HCl / palladium on carbon / ethanol / 3 h / 2482.3 Torr

2: aq. acetic acid / 1.) 0 deg C, 2.) room temperature, 17 h

3: 80 percent / pyridine / 1 h / Ambient temperature

4: 20 percent / dimethylformamide / 24 h / 90 - 100 °C

5: 42 percent / NaHCO₃ / dimethylformamide / 2 h / Ambient temperature

With hydrogenchloride; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In pyridine; ethanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00119a012