2-methyl-1-vinylcyclohexyl acetates

Base Information

• Chemical Name: 2-methyl-1-vinylcyclohexyl acetates
• CAS No.: 101568-57-4
• Molecular Formula: C₁₁H₁₈O₂
• Molecular Weight: 182.263
• Mol file: 101568-57-4.mol

Synonyms:2-methyl-1-vinylcyclohexyl acetates

Chemical Property of 2-methyl-1-vinylcyclohexyl acetates

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-methyl-1-vinylcyclohexyl acetates

There total 5 articles about 2-methyl-1-vinylcyclohexyl acetates which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Methylcyclohexanone (583-60-8) → 2-methyl-1-vinylcyclohexyl acetates (101568-57-4)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 0 °C

2: 0 °C

In tetrahydrofuran;

DOI:10.1016/S0040-4020(01)91131-7

Reference yield:

2-methyl-1-vinylcyclohexan-1-ol (6331-99-3) + acetic anhydride (108-24-7) → 2-methyl-1-vinylcyclohexyl acetates (101568-57-4)

Guidance literature:

at 0 ℃;

DOI:10.1016/S0040-4020(01)91131-7

Reference yield:

→ (+/-)-1r-acetoxy-2t-methyl-1-vinyl-cyclohexane (67902-66-3,67902-67-4,101568-57-4)

Guidance literature:

With methanol; palladium on activated charcoal; Lindlar's catalyst; Hydrogenation;

upstream raw materials:

(+/-)-1r-acetoxy-1-ethynyl-2c-methyl-cyclohexane

cis-1-ethynyl-2-methylcyclohexan-ol

2-methyl-1-vinylcyclohexan-1-ol

acetic anhydride

Downstream raw materials:

(+/-)-1-((E)-2-acetoxy-ethylidene)-2-methyl-cyclohexane