(1,3-bis(dicyclohexylphosphino)propane)dimethylpalladium(II)

Base Information

• Chemical Name: (1,3-bis(dicyclohexylphosphino)propane)dimethylpalladium(II)
• CAS No.: 343987-36-0
• Molecular Formula: C₂₉H₅₆P₂Pd
• Molecular Weight: 573.131
• Mol file: 343987-36-0.mol

Synonyms:(1,3-bis(dicyclohexylphosphino)propane)dimethylpalladium(II)

Chemical Property of (1,3-bis(dicyclohexylphosphino)propane)dimethylpalladium(II)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1,3-bis(dicyclohexylphosphino)propane)dimethylpalladium(II)

There total 1 articles about (1,3-bis(dicyclohexylphosphino)propane)dimethylpalladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

(N,N,N',N'-tetramethylethylenediamine)dimethylpalladium(II) + 1,3-bis(dicyclohexylphosphine)propane (103099-52-1) → (1,3-bis(dicyclohexylphosphino)propane)dimethylpalladium(II) (343987-36-0)

Guidance literature:

In benzene; at room temp.; characterized by spectroscopic data;

DOI:10.1021/ja0056062

Reference yield: 100.0%

xenon difluoride (13709-36-9) + (1,3-bis(dicyclohexylphosphino)propane)dimethylpalladium(II) (343987-36-0) → [PdF2(di(cyclohexylphosphino)propane)] (630406-97-2)

Guidance literature:

In dichloromethane; byproducts: C2H6, Xe; Pd dimethyl complex was treated with an equiv. of XeF2 in dry CH2Cl2; -30°C - room temp.; triturating of concd. CH2Cl2 soln. with pentane;

DOI:10.1021/ja0377753

upstream raw materials:

1,3-bis(dicyclohexylphosphine)propane

Downstream raw materials:

[PdF₂(di(cyclohexylphosphino)propane)]