N-(3-(2-(2H-tetrazol-5-yl)ethyl)phenethyl)-4-chlorobenzenesulfonamide

Base Information

Chemical Name:N-(3-(2-(2H-tetrazol-5-yl)ethyl)phenethyl)-4-chlorobenzenesulfonamide
CAS No.:1333145-01-9
Molecular Formula:C₁₇H₁₈ClN₅O₂S
Molecular Weight:391.881
Hs Code.:

Synonyms:N-(3-(2-(2H-tetrazol-5-yl)ethyl)phenethyl)-4-chlorobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-(2-(2H-tetrazol-5-yl)ethyl)phenethyl)-4-chlorobenzenesulfonamide

Chemical Property:

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Technology Process of N-(3-(2-(2H-tetrazol-5-yl)ethyl)phenethyl)-4-chlorobenzenesulfonamide

There total 8 articles about N-(3-(2-(2H-tetrazol-5-yl)ethyl)phenethyl)-4-chlorobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1333145-08-6
4-chloro-N-(3-(2-cyanoethyl)phenethyl)benzenesulfonamide

: 1333145-01-9
N-(3-(2-(2H-tetrazol-5-yl)ethyl)phenethyl)-4-chlorobenzenesulfonamide

Guidance literature:: With sodium azide; zinc dibromide; In water; at 130 ℃; for 12h; Microwave irradiation;
DOI:10.1021/jm200980u

Reference yield:

: 1333145-07-5
ethyl 3-(3-(2-(4-chlorophenylsulfonamido)ethyl)phenyl)propanoate

: 1333145-01-9
N-(3-(2-(2H-tetrazol-5-yl)ethyl)phenethyl)-4-chlorobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / dichloromethane / 3 h / -78 - 0 °C

2: ammonia; iodine / water / 20 h / 60 °C

3: sodium azide; zinc dibromide / water / 12 h / 130 °C / Microwave irradiation

With sodium azide; ammonia; iodine; diisobutylaluminium hydride; zinc dibromide; In dichloromethane; water;
DOI:10.1021/jm200980u

Reference yield:

: 1333145-05-3
(E)-ethyl 3-(3-(2-(((benzyloxy)carbonyl)amino)ethyl)phenyl)acrylate

: 1333145-01-9
N-(3-(2-(2H-tetrazol-5-yl)ethyl)phenethyl)-4-chlorobenzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C

2: triethylamine / dichloromethane / 1 h / 20 °C

3: diisobutylaluminium hydride / dichloromethane / 3 h / -78 - 0 °C

4: ammonia; iodine / water / 20 h / 60 °C

5: sodium azide; zinc dibromide / water / 12 h / 130 °C / Microwave irradiation

With sodium azide; palladium 10% on activated carbon; ammonia; hydrogen; iodine; diisobutylaluminium hydride; triethylamine; zinc dibromide; In methanol; dichloromethane; water;
DOI:10.1021/jm200980u