piperidinium 1-tert-butoxycarbonyl-5-[2-cyano-2-(N'-phenylhydrazinocarbonyl)-vinyl]-6-oxo-1,2,3,6-tetrahydropyridin-4-olate

Base Information

Chemical Name:piperidinium 1-tert-butoxycarbonyl-5-[2-cyano-2-(N'-phenylhydrazinocarbonyl)-vinyl]-6-oxo-1,2,3,6-tetrahydropyridin-4-olate
CAS No.:1296688-28-2
Molecular Formula:C₅H₁₁N*C₂₀H₂₂N₄O₅
Molecular Weight:483.568
Hs Code.:

Synonyms:piperidinium 1-tert-butoxycarbonyl-5-[2-cyano-2-(N'-phenylhydrazinocarbonyl)-vinyl]-6-oxo-1,2,3,6-tetrahydropyridin-4-olate

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Chemical Property of piperidinium 1-tert-butoxycarbonyl-5-[2-cyano-2-(N'-phenylhydrazinocarbonyl)-vinyl]-6-oxo-1,2,3,6-tetrahydropyridin-4-olate

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Technology Process of piperidinium 1-tert-butoxycarbonyl-5-[2-cyano-2-(N'-phenylhydrazinocarbonyl)-vinyl]-6-oxo-1,2,3,6-tetrahydropyridin-4-olate

There total 2 articles about piperidinium 1-tert-butoxycarbonyl-5-[2-cyano-2-(N'-phenylhydrazinocarbonyl)-vinyl]-6-oxo-1,2,3,6-tetrahydropyridin-4-olate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-89-4
piperidine

: C₁₃H₂₀N₂O₄

: 60598-59-6
cyanoacetic acid N-phenylhydrazide

: 1296688-28-2
piperidinium 1-tert-butoxycarbonyl-5-[2-cyano-2-(N'-phenylhydrazinocarbonyl)-vinyl]-6-oxo-1,2,3,6-tetrahydropyridin-4-olate

Guidance literature:: In isopropyl alcohol; at 20 ℃;
DOI:10.1016/j.tet.2011.02.052

Reference yield:

: 845267-78-9
tert-butyl 2,4-dioxopiperidine-1-carboxylate

: 1296688-28-2
piperidinium 1-tert-butoxycarbonyl-5-[2-cyano-2-(N'-phenylhydrazinocarbonyl)-vinyl]-6-oxo-1,2,3,6-tetrahydropyridin-4-olate

Guidance literature:: Multi-step reaction with 2 steps

1: 0.08 h / 20 °C

2: isopropyl alcohol / 20 °C

In isopropyl alcohol;
DOI:10.1016/j.tet.2011.02.052