2-(N-tert-butoxycarbonyl-S-benzylcysteine)-4-(1-hydroxymethyl)thiazole

Base Information

Chemical Name:2-(N-tert-butoxycarbonyl-S-benzylcysteine)-4-(1-hydroxymethyl)thiazole
CAS No.:1027259-00-2
Molecular Formula:C₁₈H₂₄N₂O₃S₂
Molecular Weight:380.532
Hs Code.:

Synonyms:2-(N-tert-butoxycarbonyl-S-benzylcysteine)-4-(1-hydroxymethyl)thiazole

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Chemical Property of 2-(N-tert-butoxycarbonyl-S-benzylcysteine)-4-(1-hydroxymethyl)thiazole

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Technology Process of 2-(N-tert-butoxycarbonyl-S-benzylcysteine)-4-(1-hydroxymethyl)thiazole

There total 6 articles about 2-(N-tert-butoxycarbonyl-S-benzylcysteine)-4-(1-hydroxymethyl)thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1027245-62-0
ethyl N-tert-butoxycarbonyl-S-benzylcysteine-4-thiazolecarboxylate

: 1027259-00-2
2-(N-tert-butoxycarbonyl-S-benzylcysteine)-4-(1-hydroxymethyl)thiazole

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 25 ℃; for 4h;
DOI:10.1002/jhet.5570320436

Reference yield:

: 5068-28-0
(2R)-3-benzylsulfanyl-2-tert-butoxycarbonylamino-propionic acid

: 1027259-00-2
2-(N-tert-butoxycarbonyl-S-benzylcysteine)-4-(1-hydroxymethyl)thiazole

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / 1,3-dicyclohexylcarbodiimide, NH₃ (gas) / CH₂Cl₂ / 3 h / 25 °C

2: 96 percent / Lawesson's reagent / tetrahydrofuran / 4 h / 25 °C

3: 63 percent / tetrahydrofuran / 4 h / 25 °C

4: 96 percent / LiAlH₄ / tetrahydrofuran / 4 h / 25 °C

With Lawessons reagent; lithium aluminium tetrahydride; ammonia; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/jhet.5570320436

Reference yield:

: 3054-01-1,25988-62-9
S-benzyl-L-cysteine

: 1027259-00-2
2-(N-tert-butoxycarbonyl-S-benzylcysteine)-4-(1-hydroxymethyl)thiazole

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / Et₃N / H₂O; dioxane / 4 h

2: 97 percent / 1,3-dicyclohexylcarbodiimide, NH₃ (gas) / CH₂Cl₂ / 3 h / 25 °C

3: 96 percent / Lawesson's reagent / tetrahydrofuran / 4 h / 25 °C

4: 63 percent / tetrahydrofuran / 4 h / 25 °C

5: 96 percent / LiAlH₄ / tetrahydrofuran / 4 h / 25 °C

With Lawessons reagent; lithium aluminium tetrahydride; ammonia; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1002/jhet.5570320436