Technology Process of C43H64N6O11
There total 10 articles about C43H64N6O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C25H35N3O7;
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
for 0.0833333h;
Inert atmosphere;
C18H31N3O5;
In
dichloromethane;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1007/s00726-011-0912-4
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h / Inert atmosphere
1.2: 2 h / 20 °C / Inert atmosphere
2.1: water; lithium hydroxide / tetrahydrofuran
3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h / Inert atmosphere
3.2: 2 h / 20 °C / Inert atmosphere
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1007/s00726-011-0912-4
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: palladium 10% on activated carbon; ammonium formate / methanol / Reflux
2.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h / Inert atmosphere
2.2: 2 h / 20 °C / Inert atmosphere
With
palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonium formate; N-ethyl-N,N-diisopropylamine;
In
methanol; dichloromethane;
DOI:10.1007/s00726-011-0912-4
