(hex-5-yn-1-yl) (3R,4R,5S)-4-acetamido-5-amino-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonic acid

Base Information

Chemical Name:(hex-5-yn-1-yl) (3R,4R,5S)-4-acetamido-5-amino-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonic acid
CAS No.:1332499-15-6
Molecular Formula:C₁₉H₃₃N₂O₅P
Molecular Weight:400.455
Hs Code.:

Synonyms:(hex-5-yn-1-yl) (3R,4R,5S)-4-acetamido-5-amino-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonic acid

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Chemical Property of (hex-5-yn-1-yl) (3R,4R,5S)-4-acetamido-5-amino-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonic acid

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Technology Process of (hex-5-yn-1-yl) (3R,4R,5S)-4-acetamido-5-amino-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonic acid

There total 6 articles about (hex-5-yn-1-yl) (3R,4R,5S)-4-acetamido-5-amino-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1356826-66-8
C₂₄H₄₁N₂O₇P

: 1332499-15-6
(hex-5-yn-1-yl) (3R,4R,5S)-4-acetamido-5-amino-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonic acid

Guidance literature:: With trifluoroacetic acid; In 1,4-dioxane; water;
DOI:10.1039/c1ob05384a

Reference yield:

: 1332499-12-3
methyl (hex-5-yn-1-yl) [(3R,4R,5S)-4-acetamido-5-(1,1-dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate]

: 1332499-15-6
(hex-5-yn-1-yl) (3R,4R,5S)-4-acetamido-5-amino-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium iodide / acetone / 24 h / Reflux; Inert atmosphere

2: trifluoroacetic acid / 1,4-dioxane; water

With trifluoroacetic acid; sodium iodide; In 1,4-dioxane; water; acetone;
DOI:10.1039/c1ob05384a

Reference yield:

: C₆H₁₅N*C₁₉H₃₅N₂O₇P

: 1332499-15-6
(hex-5-yn-1-yl) (3R,4R,5S)-4-acetamido-5-amino-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 1 h / Inert atmosphere

2: sodium iodide / acetone / 24 h / Reflux; Inert atmosphere

3: trifluoroacetic acid / 1,4-dioxane; water

With trifluoroacetic acid; sodium iodide; In 1,4-dioxane; water; acetone; acetonitrile;
DOI:10.1039/c1ob05384a