methyl (hex-5-yn-1-yl) [(3R,4R,5S)-4-acetamido-5-(1,1-dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate]

Base Information

Chemical Name:methyl (hex-5-yn-1-yl) [(3R,4R,5S)-4-acetamido-5-(1,1-dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate]
CAS No.:1332499-12-3
Molecular Formula:C₂₅H₄₃N₂O₇P
Molecular Weight:514.599
Hs Code.:

Synonyms:methyl (hex-5-yn-1-yl) [(3R,4R,5S)-4-acetamido-5-(1,1-dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate]

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Chemical Property of methyl (hex-5-yn-1-yl) [(3R,4R,5S)-4-acetamido-5-(1,1-dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate]

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Technology Process of methyl (hex-5-yn-1-yl) [(3R,4R,5S)-4-acetamido-5-(1,1-dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate]

There total 3 articles about methyl (hex-5-yn-1-yl) [(3R,4R,5S)-4-acetamido-5-(1,1-dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1158845-35-2
ammonium [methyl (3R,4R,5S)-4-acetamido-5-(1,1-dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate]

: 1332499-12-3
methyl (hex-5-yn-1-yl) [(3R,4R,5S)-4-acetamido-5-(1,1-dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate]

Guidance literature:: Multi-step reaction with 2 steps

1: Amberlite IR-120 / water

2: acetonitrile / 1 h / Inert atmosphere

With Amberlite IR-120; In water; acetonitrile;
DOI:10.1039/c1ob05384a

Reference yield:

: 928-90-5
5-hexyl-1-ol

: 1332499-12-3
methyl (hex-5-yn-1-yl) [(3R,4R,5S)-4-acetamido-5-(1,1-dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate]

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-dimethylpyridine / dichloromethane / 1 h / -60 °C / Inert atmosphere

2: acetonitrile / 1 h / Inert atmosphere

With 2,6-dimethylpyridine; In dichloromethane; acetonitrile;
DOI:10.1039/c1ob05384a