5-(2-(benzyloxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)-1H-tetrazole

Base Information

Chemical Name:5-(2-(benzyloxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)-1H-tetrazole
CAS No.:1448816-38-3
Molecular Formula:C₂₄H₂₄N₄O₅
Molecular Weight:448.478
Hs Code.:

Synonyms:5-(2-(benzyloxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)-1H-tetrazole

Suppliers and Price of 5-(2-(benzyloxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)-1H-tetrazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-(2-(benzyloxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)-1H-tetrazole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-(2-(benzyloxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)-1H-tetrazole

There total 8 articles about 5-(2-(benzyloxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₂₄ClNO₅

: 1448816-38-3
5-(2-(benzyloxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)-1H-tetrazole

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 60 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.bmcl.2013.06.004

Reference yield:

: 1448816-33-8
2-(benzyloxy)-4-methoxy-N-(3,4,5-trimethoxyphenyl)benzamide

: 1448816-38-3
5-(2-(benzyloxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)-1H-tetrazole

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 4 h / 60 °C / Inert atmosphere

With pyridine; sodium azide; oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.004

Reference yield:

: 100-39-0
benzyl bromide

: 1448816-38-3
5-(2-(benzyloxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)-1H-tetrazole

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / N,N-dimethyl-formamide / Inert atmosphere

2: sodium hydroxide; water / 1,4-dioxane / Inert atmosphere

3: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C / Inert atmosphere

4: triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

5: oxalyl dichloride; pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere

6: sodium azide / N,N-dimethyl-formamide / 4 h / 60 °C / Inert atmosphere

With pyridine; sodium azide; oxalyl dichloride; water; potassium carbonate; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.004