(2S,3R)-3-(diphenylphosphorylamino)-N,N,2-trimethyl-3-phenylpropanethioamide

Base Information

Chemical Name:(2S,3R)-3-(diphenylphosphorylamino)-N,N,2-trimethyl-3-phenylpropanethioamide
CAS No.:1182707-47-6
Molecular Formula:C₂₄H₂₇N₂OPS
Molecular Weight:422.531
Hs Code.:

Synonyms:(2S,3R)-3-(diphenylphosphorylamino)-N,N,2-trimethyl-3-phenylpropanethioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-3-(diphenylphosphorylamino)-N,N,2-trimethyl-3-phenylpropanethioamide

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Technology Process of (2S,3R)-3-(diphenylphosphorylamino)-N,N,2-trimethyl-3-phenylpropanethioamide

There total 1 articles about (2S,3R)-3-(diphenylphosphorylamino)-N,N,2-trimethyl-3-phenylpropanethioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5309-94-4
N,N-Dimethyl-thiopropionamide

: 98837-46-8,67764-52-7
P,P-diphenyl-N-(phenylmethylene)phosphinic amide

: (2R,3S)-3-(diphenylphosphorylamino)-N,N,2-trimethyl-3-phenylpropanethioamide

: 1182707-47-6
(2S,3R)-3-(diphenylphosphorylamino)-N,N,2-trimethyl-3-phenylpropanethioamide

: (2S,3R)-3-(diphenylphosphorylamino)-N,N,2-trimethyl-3-phenylpropanethioamide

Guidance literature:: P,P-diphenyl-N-(phenylmethylene)phosphinic amide; With tetrakis(actonitrile)copper(I) hexafluorophosphate; (R,R)-1,2-bis(2,5-diphenylphospholanyl)ethane; In tetrahydrofuran; toluene; at 20 ℃; Inert atmosphere;

N,N-Dimethyl-thiopropionamide; With lithium o-methoxyphenoxide; In tetrahydrofuran; toluene; at -20 ℃; for 72h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.200901588