C₂₂H₃₀O₅

Base Information

Chemical Name:C₂₂H₃₀O₅
CAS No.:1363407-74-2
Molecular Formula:C₂₂H₃₀O₅
Molecular Weight:374.477
Hs Code.:

C<sub>22</sub>H<sub>30</sub>O<sub>5</sub>

Synonyms:C₂₂H₃₀O₅

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Chemical Property of C₂₂H₃₀O₅

Chemical Property:

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Technology Process of C₂₂H₃₀O₅

There total 12 articles about C₂₂H₃₀O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6728-26-3
(E)-2-Hexenal

: 1363407-74-2
C₂₂H₃₀O₅

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran / 0.25 h / -20 °C / Inert atmosphere

2: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / dichloromethane / 18 h / -20 °C / Molecular sieve; Inert atmosphere

3: titanium(IV) isopropylate / dichloromethane / 0.25 h / Inert atmosphere

4: dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

5: dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

6: Grubbs catalyst first generation / toluene / 36 h / Inert atmosphere; Reflux

With Grubbs catalyst first generation; titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; In tetrahydrofuran; dichloromethane; toluene; 2: Sharpless epoxidation / 3: Sharpless dihydroxylation;
DOI:10.1021/jo202199g

Reference yield:

: 928-95-0
(E)-2-Hexen-1-ol

: 1363407-74-2
C₂₂H₃₀O₅

Guidance literature:: Multi-step reaction with 7 steps

1: dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane / 1 h / 0 °C / Inert atmosphere

2: tetrahydrofuran / 0.25 h / -20 °C / Inert atmosphere

3: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / dichloromethane / 18 h / -20 °C / Molecular sieve; Inert atmosphere

4: titanium(IV) isopropylate / dichloromethane / 0.25 h / Inert atmosphere

5: dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

6: dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

7: Grubbs catalyst first generation / toluene / 36 h / Inert atmosphere; Reflux

With Grubbs catalyst first generation; titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; toluene; 3: Sharpless epoxidation / 4: Sharpless dihydroxylation;
DOI:10.1021/jo202199g

Reference yield:

: 1335029-07-6
(R)-1-(((2-(benzyloxy)hex-5-en-1-yl)oxy)methyl)-4-methoxybenzene

: 1363407-74-2
C₂₂H₃₀O₅

Guidance literature:: Multi-step reaction with 4 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 1 h / 0 - 20 °C

2: dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 1 h / 0 °C / Inert atmosphere; Reflux

3: dmap; dicyclohexyl-carbodiimide / Inert atmosphere

4: Grubbs catalyst first generation / toluene / 36 h / Inert atmosphere; Reflux

With Grubbs catalyst first generation; dmap; dimethyl sulfoxide; dicyclohexyl-carbodiimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dichloromethane; water; ethyl acetate; toluene;
DOI:10.1021/jo202199g