2,4-Dihydroxybenzoic acid 2-[(5-nitro-2-furanyl)methylene]hydrazide

Base Information

Chemical Name:2,4-Dihydroxybenzoic acid 2-[(5-nitro-2-furanyl)methylene]hydrazide
CAS No.:304481-57-0
Molecular Formula:C₁₂H₉N₃O₆
Molecular Weight:291.22
Hs Code.:
DSSTox Substance ID:DTXSID801162019

Synonyms:DTXSID801162019;2,4-Dihydroxybenzoic acid 2-[(5-nitro-2-furanyl)methylene]hydrazide;304481-57-0

Suppliers and Price of 2,4-Dihydroxybenzoic acid 2-[(5-nitro-2-furanyl)methylene]hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-Dihydroxybenzoic acid 2-[(5-nitro-2-furanyl)methylene]hydrazide

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:3
Exact Mass:291.04913502
Heavy Atom Count:21
Complexity:424

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C=C1O)O)C(=O)NN=CC2=CC=C(O2)[N+](=O)[O-]

Technology Process of 2,4-Dihydroxybenzoic acid 2-[(5-nitro-2-furanyl)methylene]hydrazide

There total 4 articles about 2,4-Dihydroxybenzoic acid 2-[(5-nitro-2-furanyl)methylene]hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13221-86-8
2,4-dihydroxybenzoic acid hydrazide

: 5-nitro-2-furaldehyde diacetate

: 304481-57-0
C₁₂H₉N₃O₆

: 736-53-8
1,2-bis((5-nitrofuran-2-yl)methylene)hydrazine

Guidance literature:: 5-nitro-2-furaldehyde diacetate; With sulfuric acid; In water; at 100 ℃;

2,4-dihydroxybenzoic acid hydrazide; In water; at 100 ℃;
DOI:10.1016/j.molliq.2021.116911

Reference yield:

: 57438-38-7
2,4-dihydroxybenzoyl chloride

: 304481-57-0
C₁₂H₉N₃O₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: 0.5 h / 0 °C

2.1: hydrazine hydrate / ethanol / 9 h / Reflux

3.1: sulfuric acid / water / 100 °C

3.2: 100 °C

With sulfuric acid; hydrazine hydrate; In ethanol; water;
DOI:10.1016/j.molliq.2021.116911

Reference yield:

: 4143-00-4
ethyl 2,4-dihydroxybenzoate

: 304481-57-0
C₁₂H₉N₃O₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrazine hydrate / ethanol / 9 h / Reflux

2.1: sulfuric acid / water / 100 °C

2.2: 100 °C

With sulfuric acid; hydrazine hydrate; In ethanol; water;
DOI:10.1016/j.molliq.2021.116911