iso-butyl 3-(2-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

Base Information

Chemical Name:iso-butyl 3-(2-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate
CAS No.:1252813-52-7
Molecular Formula:C₂₀H₃₁BO₅
Molecular Weight:362.274
Hs Code.:

Synonyms:iso-butyl 3-(2-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of iso-butyl 3-(2-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

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Technology Process of iso-butyl 3-(2-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

There total 3 articles about iso-butyl 3-(2-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1266612-71-8
C₁₄H₁₈O₃

: 73183-34-3
bis(pinacol)diborane

: 1252813-52-7
iso-butyl 3-(2-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

Guidance literature:: With sodium t-butanolate; ((2S,3S)-6-mesityl-2,3-diphenyl-2,3,5,6-tetrahydroimidazo[1,2-c]quinazolin-5-yl)copper(I)chloride; In methanol; diethyl ether; at -55 ℃; for 6h; Product distribution / selectivity; Inert atmosphere;

Reference yield: 90.0%

: 1252813-45-8
(E)-isobutyl 3-(2-methoxyphenyl)acrylate

: 73183-34-3
bis(pinacol)diborane

: 1252813-52-7
iso-butyl 3-(2-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

Guidance literature:: With methanol; ((2S,3S)-6-mesityl-2,3-diphenyl-2,3,5,6-tetrahydroimidazo[1,2-c]quinazolin-5-yl)copper(I) chloride; sodium t-butanolate; In toluene; at -30 ℃; for 6h; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ol1021756

Reference yield:

: 1252813-45-8
(E)-isobutyl 3-(2-methoxyphenyl)acrylate

: 73183-34-3
bis(pinacol)diborane

: iso-butyl 3-(2-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

: 1252813-52-7
iso-butyl 3-(2-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

Guidance literature:: With methanol; ((2S,3S)-6-mesityl-2,3-diphenyl-2,3,5,6-tetrahydroimidazo[1,2-c]quinazolin-5-yl)copper(I) chloride; sodium t-butanolate; In toluene; at 0 ℃; for 1.66667h; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ol1021756