octyl 3,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:octyl 3,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside
CAS No.:503602-45-7
Molecular Formula:C₅₉H₆₉NO₁₂
Molecular Weight:984.196
Hs Code.:

Synonyms:octyl 3,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Chemical Property of octyl 3,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Technology Process of octyl 3,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

There total 4 articles about octyl 3,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 503602-44-6
octyl 2-O-acetyl-3,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 503602-45-7
octyl 3,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With sodium; In methanol; at 20 ℃; for 48h;
DOI:10.1016/S0008-6215(02)00178-7

Reference yield:

: 161664-93-3
octyl 4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 503602-45-7
octyl 3,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 56 percent / sodium hydride / dimethylformamide / 3 h / 20 °C

2: 96 percent / sodium cyanoborohydride; HCl; 4A molecular sieves / tetrahydrofuran; diethyl ether / 0 - 20 °C

3: 80 percent / N-iodosuccinimide; 4A molecular sieves / CH₂Cl₂ / 0 °C

4: 77 percent / sodium / methanol / 48 h / 20 °C

With hydrogenchloride; N-iodo-succinimide; 4 A molecular sieve; sodium; sodium hydride; sodium cyanoborohydride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(02)00178-7

Reference yield:

: 503602-15-1
octyl 3-O-allyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 503602-45-7
octyl 3,4,6-tri-O-benzyl-β-D-galactopyranosyl-(1->4)-3-O-allyl-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / sodium cyanoborohydride; HCl; 4A molecular sieves / tetrahydrofuran; diethyl ether / 0 - 20 °C

2: 80 percent / N-iodosuccinimide; 4A molecular sieves / CH₂Cl₂ / 0 °C

3: 77 percent / sodium / methanol / 48 h / 20 °C

With hydrogenchloride; N-iodo-succinimide; 4 A molecular sieve; sodium; sodium cyanoborohydride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1016/S0008-6215(02)00178-7