(7,8-dihydro-5,10,15,20-tetraphenylporphyrin) iron(III) chloride

Base Information

• Chemical Name: (7,8-dihydro-5,10,15,20-tetraphenylporphyrin) iron(III) chloride
• CAS No.: 94483-24-6
• Molecular Formula: C₄₄H₃₀ClFeN₄
• Molecular Weight: 706.049
• Mol file: 94483-24-6.mol

Synonyms:(7,8-dihydro-5,10,15,20-tetraphenylporphyrin) iron(III) chloride

Chemical Property of (7,8-dihydro-5,10,15,20-tetraphenylporphyrin) iron(III) chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (7,8-dihydro-5,10,15,20-tetraphenylporphyrin) iron(III) chloride

There total 4 articles about (7,8-dihydro-5,10,15,20-tetraphenylporphyrin) iron(III) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

iron(II) chloride tetrahydrate + (7,8-dihydro-5,10,15,20-tetraphenylporphyrin) cadmium (II) (202007-67-8) → (7,8-dihydro-5,10,15,20-tetraphenylporphyrin) iron(III) chloride (94483-24-6)

Guidance literature:

With sodium ascorbate; In acetone; at 60 ℃; for 2h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.ica.2013.01.012

Reference yield: 75.0%

iron(II) chloride tetrahydrate + 7,8-dihydro-5,10,15,20-tetraphenylporphyrin → meso-tetraphenylporphyrin iron(III) chloride (16456-81-8,170645-84-8) + (7,8-dihydro-5,10,15,20-tetraphenylporphyrin) iron(III) chloride (94483-24-6)

Guidance literature:

In N,N-dimethyl-formamide; Reflux;

DOI:10.1016/j.ica.2013.01.012

Reference yield:

(Fe(TPC))2(μ-O) → (7,8-dihydro-5,10,15,20-tetraphenylporphyrin) iron(III) chloride (94483-24-6)

Guidance literature:

With hydrogenchloride; In hydrogenchloride; 0.1 M aq. HCl;

DOI:10.1021/ja00218a002

upstream raw materials:

(7,8-dihydro-5,10,15,20-tetraphenylporphyrin) cadmium (II)

Downstream raw materials:

Fe(5,10,15,20-tetraphenyl-chlorin)

?(7,8-dihydro-5,10,15,20-tetraphenylporphyrin) iron(II) bis-(tert-butyl)isocyanide

[(5,10,15,20-tetraphenylchlorin^(2-))Fe(2-methylimidazole)2]Cl

[(tetraphenylchlorinato)iron(III)(CN)2]NBu₄