tetrakis(phenyl)chlorinatoiron(III) trifluorosulfonate

Base Information

Chemical Name:tetrakis(phenyl)chlorinatoiron(III) trifluorosulfonate
CAS No.:352515-78-7
Molecular Formula:CF₃O₃S*C₄₄H₃₀FeN₄
Molecular Weight:819.666
Hs Code.:

Synonyms:

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Chemical Property of tetrakis(phenyl)chlorinatoiron(III) trifluorosulfonate

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Technology Process of tetrakis(phenyl)chlorinatoiron(III) trifluorosulfonate

There total 2 articles about tetrakis(phenyl)chlorinatoiron(III) trifluorosulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 94483-24-6
(7,8-dihydro-5,10,15,20-tetraphenylporphyrin) iron(III) chloride

: 2923-28-6
silver trifluoromethanesulfonate

: 352515-78-7
(tetraphenylchlorinato)iron(III) trifluoromethanesulfonate

Guidance literature:: In tetrahydrofuran; under Ar; stirring at 60°C for 15 min; filtered; hexane added gradually; after standing overnight, crystals collected; elem. anal.;
DOI:10.1039/b100925g

Reference yield: 70.0%

: 94483-24-6
(7,8-dihydro-5,10,15,20-tetraphenylporphyrin) iron(III) chloride

: 2923-28-6
silver trifluoromethanesulfonate

: 352515-78-7
tetrakis(phenyl)chlorinatoiron(III) trifluorosulfonate

Guidance literature:: In tetrahydrofuran;
DOI:10.1021/ic0013328

Reference yield: 85.0%

: 2946-61-4
phenylphosphonous acid dimethyl ester

: 352515-78-7
tetrakis(phenyl)chlorinatoiron(III) trifluorosulfonate

: bis(dimethylphenylphosphonite)tetrakis(phenyl)chlorinatoiron(III) trifluorosulfonate

Guidance literature:: In dichloromethane; under Ar; to a soln. of Fe-contg. compd. (0.09 mmol) in CH2Cl2 was addedP(OMe)2Ph (0.23 mmol) under stirring at room temp.; after stirring for 15 min, the soln. became green;; toluene and pentane were added and the soln. was set aside overnight forcrystn. at 0°C; crystals were collected by filtration and washed with hexane;
DOI:10.1016/S0020-1693(02)01192-1