(2S,4aS,7R,8aR)-3-Benzyl-2,4,4,7-tetramethyl-octahydro-benzo[e][1,3]oxazine

Base Information

Chemical Name:(2S,4aS,7R,8aR)-3-Benzyl-2,4,4,7-tetramethyl-octahydro-benzo[e][1,3]oxazine
CAS No.:134046-25-6
Molecular Formula:C₁₉H₂₉NO
Molecular Weight:287.445
Hs Code.:

Synonyms:(2S,4aS,7R,8aR)-3-Benzyl-2,4,4,7-tetramethyl-octahydro-benzo[e][1,3]oxazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4aS,7R,8aR)-3-Benzyl-2,4,4,7-tetramethyl-octahydro-benzo[e][1,3]oxazine

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Technology Process of (2S,4aS,7R,8aR)-3-Benzyl-2,4,4,7-tetramethyl-octahydro-benzo[e][1,3]oxazine

There total 1 articles about (2S,4aS,7R,8aR)-3-Benzyl-2,4,4,7-tetramethyl-octahydro-benzo[e][1,3]oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 75-07-0,9002-91-9
acetaldehyde

: 2-(1-Benzylamino-1-methyl-ethyl)-5-methyl-cyclohexanol

: 134046-25-6
(2S,4aS,7R,8aR)-3-Benzyl-2,4,4,7-tetramethyl-octahydro-benzo[e][1,3]oxazine

Guidance literature:: In toluene; Heating;
DOI:10.1021/jo960047w

Reference yield:

: 134046-25-6
(2S,4aS,7R,8aR)-3-Benzyl-2,4,4,7-tetramethyl-octahydro-benzo[e][1,3]oxazine

: 931-50-0
cyclohexylmagnesium bromide

: 8-[N-benzyl-N-((R)-1-cyclohexylethyl)amino]menthol

: 8-[N-benzyl-N-((S)-1-cyclohexylethyl)amino]menthol

Guidance literature:: In benzene; at 78 ℃; Yield given. Yields of byproduct given;
DOI:10.1021/jo960047w

Reference yield:

: 134046-25-6
(2S,4aS,7R,8aR)-3-Benzyl-2,4,4,7-tetramethyl-octahydro-benzo[e][1,3]oxazine

: Benzyl-((S)-1-cyclopropyl-ethyl)-amine; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 78 °C

2: 68 percent / P₂O₅ / toluene / 2 h / Heating

With phosphorus pentoxide; In toluene; benzene;
DOI:10.1021/jo960047w