12-hydroxydodecyl 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

Base Information

Chemical Name:12-hydroxydodecyl 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside
CAS No.:321873-10-3
Molecular Formula:C₇₃H₇₄O₁₉
Molecular Weight:1255.38
Hs Code.:

Synonyms:12-hydroxydodecyl 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

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Chemical Property of 12-hydroxydodecyl 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

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Technology Process of 12-hydroxydodecyl 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

There total 1 articles about 12-hydroxydodecyl 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 5675-51-4
1,12-dodecandiol

: C₆₁H₄₉BrO₁₇

: 321873-10-3
12-hydroxydodecyl 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; silver trifluoromethanesulfonate; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1016/S0008-6215(00)00238-X

Reference yield:

: 321873-10-3
12-hydroxydodecyl 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

: 12-azidododecyl 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 4 h / 20 °C

2: NaN₃ / dimethylformamide / 16 h / 20 - 60 °C

With pyridine; sodium azide; In N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)00238-X