2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

Base Information

Chemical Name:2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside
CAS No.:174149-23-6
Molecular Formula:C₃₂H₃₆O₈Si
Molecular Weight:576.719
Hs Code.:

Synonyms:2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

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Technology Process of 2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

There total 4 articles about 2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 98-88-4
benzoyl chloride

: 117253-03-9
2-(trimethylsilyl)ethyl 4,6-O-benzylidene-β-D-glucopyranoside

: 174149-23-6
2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

Guidance literature:: With dmap; In pyridine; at 25 ℃; for 2h;
DOI:10.1021/jo951067l

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 174149-23-6
2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / PTSA / acetonitrile / 3 h / 25 °C

2: 96 percent / DMAP / pyridine / 2 h / 25 °C

With dmap; toluene-4-sulfonic acid; In pyridine; acetonitrile;
DOI:10.1021/jo951067l

Reference yield:

: 81342-44-1
(2R,3R,4S,5R,6R)-2-(acetoxymethyl)-6-(2-(trimethylsilyl)ethoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 174149-23-6
2-(trimethylsilyl)ethyl 2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: Amberlite IRA 910 / methanol / 2 h / 25 °C

2: 89 percent / PTSA / acetonitrile / 3 h / 25 °C

3: 96 percent / DMAP / pyridine / 2 h / 25 °C

With dmap; Amberlite IRA 910; toluene-4-sulfonic acid; In pyridine; methanol; acetonitrile;
DOI:10.1021/jo951067l