15,16-bis[(4-nitrophenoxy)methyl]-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecine

Base Information

• Chemical Name: 15,16-bis[(4-nitrophenoxy)methyl]-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecine
• CAS No.: 134046-51-8
• Molecular Formula: C₂₈H₃₀N₂O₁₁
• Molecular Weight: 570.553

Synonyms:15,16-bis[(4-nitrophenoxy)methyl]-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecine

Chemical Property of 15,16-bis[(4-nitrophenoxy)methyl]-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecine

Chemical Property:

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Technology Process of 15,16-bis[(4-nitrophenoxy)methyl]-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecine

There total 1 articles about 15,16-bis[(4-nitrophenoxy)methyl]-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + 2,3-bis-(bromomethyl)-6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17,-pentaoxabenzocyclopentadecene (128639-28-1) → 15,16-bis[(4-nitrophenoxy)methyl]-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecine (134046-51-8)

Guidance literature:

4-nitro-phenol; With sodium hydroxide; In N,N-dimethyl-formamide; for 1h;

2,3-bis-(bromomethyl)-6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17,-pentaoxabenzocyclopentadecene; In N,N-dimethyl-formamide; for 24h; Reflux;

DOI:10.1002/hc.21134

Reference yield: 63.0%

15,16-bis[(4-nitrophenoxy)methyl]-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecine (134046-51-8) → C28H30N2NaO11(1+)*ClO4(1-) (1613310-87-4)

Guidance literature:

With sodium perchlorate; In ethanol; for 2h; Reflux;

DOI:10.1002/hc.21134

Reference yield: 56.0%

15,16-bis[(4-nitrophenoxy)methyl]-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecine (134046-51-8) → [3-({16-[(4-aminophenoxy)methyl]-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl}methoxy)phenyl]amineo-aminbenzo-15-crown-5 (1613310-82-9)

Guidance literature:

With palladium 10% on activated carbon; hydrazine hydrate; In ethanol; at 70 ℃; Reflux;

DOI:10.1002/hc.21134

upstream raw materials:

4-nitro-phenol

2,3-bis-(bromomethyl)-6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17,-pentaoxabenzocyclopentadecene

Downstream raw materials:

C₄₂H₄₂N₂O₉

C₄₄H₄₆N₂O₁₁

C₄₄H₄₆N₂O₁₁

C₂₈H₃₀N₂NaO₁₁⁽¹⁺⁾*ClO₄^(1-)

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