2a-dimethylamino-2,2-diphenyl-2,2a-dihydro-4H-azeto[2,1-b]benzo[e][1,3]thiazepine-1,9-dione

Base Information

Chemical Name:2a-dimethylamino-2,2-diphenyl-2,2a-dihydro-4H-azeto[2,1-b]benzo[e][1,3]thiazepine-1,9-dione
CAS No.:40819-24-7
Molecular Formula:C₂₅H₂₂N₂O₂S
Molecular Weight:414.528
Hs Code.:

2a-dimethylamino-2,2-diphenyl-2,2a-dihydro-4<i>H</i>-azeto[2,1-<i>b</i>]benzo[<i>e</i>][1,3]thiazepine-1,9-dione

Synonyms:2a-dimethylamino-2,2-diphenyl-2,2a-dihydro-4H-azeto[2,1-b]benzo[e][1,3]thiazepine-1,9-dione

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Chemical Property of 2a-dimethylamino-2,2-diphenyl-2,2a-dihydro-4H-azeto[2,1-b]benzo[e][1,3]thiazepine-1,9-dione

Chemical Property:

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Technology Process of 2a-dimethylamino-2,2-diphenyl-2,2a-dihydro-4H-azeto[2,1-b]benzo[e][1,3]thiazepine-1,9-dione

There total 2 articles about 2a-dimethylamino-2,2-diphenyl-2,2a-dihydro-4H-azeto[2,1-b]benzo[e][1,3]thiazepine-1,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 525-06-4
diphenyl ketene

: 40819-05-4
3-dimethylamino-1H-benzo[e][1,3]thiazepin-5-one

: 40819-24-7
2a-dimethylamino-2,2-diphenyl-2,2a-dihydro-4H-azeto[2,1-b]benzo[e][1,3]thiazepine-1,9-dione

Guidance literature:: In chloroform;

Reference yield:

: 40819-28-1
2-(bromomethyl)benzoyl bromide

: 40819-24-7
2a-dimethylamino-2,2-diphenyl-2,2a-dihydro-4H-azeto[2,1-b]benzo[e][1,3]thiazepine-1,9-dione

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂CO₃ / acetone / Heating

2: CHCl₃

With sodium carbonate; In chloroform; acetone;