C₄₁H₇₁NO₂Si₂

Base Information

Chemical Name:C₄₁H₇₁NO₂Si₂
CAS No.:1313734-22-3
Molecular Formula:C₄₁H₇₁NO₂Si₂
Molecular Weight:666.191
Hs Code.:

C<sub>41</sub>H<sub>71</sub>NO<sub>2</sub>Si<sub>2</sub>

Synonyms:C₄₁H₇₁NO₂Si₂

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Chemical Property of C₄₁H₇₁NO₂Si₂

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Technology Process of C₄₁H₇₁NO₂Si₂

There total 6 articles about C₄₁H₇₁NO₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1313734-20-1
C₄₁H₇₁N₃O₃Si₂

: 1313734-22-3
C₄₁H₇₁NO₂Si₂

Guidance literature:: With triphenylphosphine; In toluene; for 3h; Reflux; Inert atmosphere;
DOI:10.1039/c1ob05324h

Reference yield:

: 916159-69-8
[(S)-2-azido-2-((4S,5R)-2,2-dioxo-5-tetradecyl-2λ⁶-[1,3,2]dioxathiolan-4-yl)ethoxy]-tert-butyldiphenylsilane

: 1313734-22-3
C₄₁H₇₁NO₂Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

2: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

3: diisobutylaluminium hydride / toluene / 1 h / -78 °C / Inert atmosphere

4: sodium tetrahydroborate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

5: triphenylphosphine / toluene / 3 h / Reflux; Inert atmosphere

With 2,6-dimethylpyridine; sodium tetrahydroborate; diisobutylaluminium hydride; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide; toluene; 5: Staudinger type reductive cyclization;
DOI:10.1039/c1ob05324h

Reference yield:

: 1313734-17-6
C₄₁H₆₈N₄O₂Si₂

: 1313734-22-3
C₄₁H₇₁NO₂Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / toluene / 1 h / -78 °C / Inert atmosphere

2: sodium tetrahydroborate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3: triphenylphosphine / toluene / 3 h / Reflux; Inert atmosphere

With sodium tetrahydroborate; diisobutylaluminium hydride; triphenylphosphine; In dichloromethane; toluene; 3: Staudinger type reductive cyclization;
DOI:10.1039/c1ob05324h