7-(4-triphenylphosphiniumbutoxy)-2-(3,4-dihydroxyphenyl)-3,5-dihydroxy-4H-chromen-4-one iodide

Base Information

Chemical Name:7-(4-triphenylphosphiniumbutoxy)-2-(3,4-dihydroxyphenyl)-3,5-dihydroxy-4H-chromen-4-one iodide
CAS No.:1233627-97-8
Molecular Formula:C₃₇H₃₂O₇P*I
Molecular Weight:746.535
Hs Code.:

Synonyms:7-(4-triphenylphosphiniumbutoxy)-2-(3,4-dihydroxyphenyl)-3,5-dihydroxy-4H-chromen-4-one iodide

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Chemical Property of 7-(4-triphenylphosphiniumbutoxy)-2-(3,4-dihydroxyphenyl)-3,5-dihydroxy-4H-chromen-4-one iodide

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Technology Process of 7-(4-triphenylphosphiniumbutoxy)-2-(3,4-dihydroxyphenyl)-3,5-dihydroxy-4H-chromen-4-one iodide

There total 5 articles about 7-(4-triphenylphosphiniumbutoxy)-2-(3,4-dihydroxyphenyl)-3,5-dihydroxy-4H-chromen-4-one iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1233627-95-6
7-(4-iodobutoxy)-2-(3,4-dihydroxyphenyl)-3,5-dihydroxy-4H-chromen-4-one

: 603-35-0
triphenylphosphine

: 1233627-97-8
7-(4-triphenylphosphiniumbutoxy)-2-(3,4-dihydroxyphenyl)-3,5-dihydroxy-4H-chromen-4-one iodide

Guidance literature:: In toluene; at 95 ℃; for 3h; Inert atmosphere;
DOI:10.3390/molecules15074722

Reference yield:

: C₂₇H₂₅ClO₁₁

: 1233627-97-8
7-(4-triphenylphosphiniumbutoxy)-2-(3,4-dihydroxyphenyl)-3,5-dihydroxy-4H-chromen-4-one iodide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; water / acetonitrile / 1 h / Reflux

2: sodium iodide / acetone / Reflux

3: 90 °C / Neat (no solvent)

With hydrogenchloride; water; sodium iodide; In acetone; acetonitrile;
DOI:10.1002/ejoc.201100573

Reference yield:

: 1233627-93-4
7-(4-chlorobutoxy)-2-(3,4-dihydroxyphenyl)-3,5-dihydroxy-4H-chromen-4-one

: 1233627-97-8
7-(4-triphenylphosphiniumbutoxy)-2-(3,4-dihydroxyphenyl)-3,5-dihydroxy-4H-chromen-4-one iodide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium iodide / acetone / Reflux

2: 90 °C / Neat (no solvent)

With sodium iodide; In acetone;
DOI:10.1002/ejoc.201100573