<5aR-(5aα,6β,9β,10α)>-5,5a,6,9-Tetrahydro-1,3,5-trimethyl-6,9-diphenylpyrido<1,2-e>purin-2,4(1H,3H)-dion

Base Information

• Chemical Name: <5aR-(5aα,6β,9β,10α)>-5,5a,6,9-Tetrahydro-1,3,5-trimethyl-6,9-diphenylpyrido<1,2-e>purin-2,4(1H,3H)-dion
• CAS No.: 79246-61-0
• Molecular Formula: C₂₄H₂₄N₄O₂
• Molecular Weight: 400.48

Synonyms:<5aR-(5aα,6β,9β,10α)>-5,5a,6,9-Tetrahydro-1,3,5-trimethyl-6,9-diphenylpyrido<1,2-e>purin-2,4(1H,3H)-dion

Chemical Property of <5aR-(5aα,6β,9β,10α)>-5,5a,6,9-Tetrahydro-1,3,5-trimethyl-6,9-diphenylpyrido<1,2-e>purin-2,4(1H,3H)-dion

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Technology Process of <5aR-(5aα,6β,9β,10α)>-5,5a,6,9-Tetrahydro-1,3,5-trimethyl-6,9-diphenylpyrido<1,2-e>purin-2,4(1H,3H)-dion

There total 2 articles about <5aR-(5aα,6β,9β,10α)>-5,5a,6,9-Tetrahydro-1,3,5-trimethyl-6,9-diphenylpyrido<1,2-e>purin-2,4(1H,3H)-dion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.5%

3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione (58-08-2,138455-22-8,95789-13-2) + trans,trans-1,4-Diphenyl-1,3-butadiene (886-65-7,538-81-8) → 8-Benzyl-3,7-dihydro-1,3,7-trimethyl-1H-purin-2,6-dion (5426-88-0) + 3,4,5,7-Tetrahydro-1,3,7-trimethyl-10-syn-phenyl-11-anti-(trans-2-phenylethenyl)-4,5-ethano-1H-purin-2,6-dion (79246-59-6) + 3,4,5,7-Tetrahydro-1,3,7-trimethyl-11-syn-phenyl-10-anti-(trans-2-phenylethenyl)-4,5-ethano-1H-purin-2,6-dion (79246-60-9) + <5aR-(5aα,6β,9β,10α)>-5,5a,6,9-Tetrahydro-1,3,5-trimethyl-6,9-diphenylpyrido<1,2-e>purin-2,4(1H,3H)-dion (79246-61-0)

Guidance literature:

In dichloromethane; for 72h; Irradiation;

Reference yield: 9.5%

3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione (58-08-2,138455-22-8,95789-13-2) + trans,trans-1,4-Diphenyl-1,3-butadiene (886-65-7,538-81-8) → 8-Benzyl-3,7-dihydro-1,3,7-trimethyl-1H-purin-2,6-dion (5426-88-0) + 3,4,5,7-Tetrahydro-1,3,7-trimethyl-10-syn-phenyl-11-anti-(trans-2-phenylethenyl)-4,5-ethano-1H-purin-2,6-dion (79246-59-6) + 3,4,5,7-Tetrahydro-1,3,7-trimethyl-11-syn-phenyl-10-anti-(trans-2-phenylethenyl)-4,5-ethano-1H-purin-2,6-dion (79246-60-9) + <5aR-(5aα,6β,9β,10α)>-5,5a,6,9-Tetrahydro-1,3,5-trimethyl-6,9-diphenylpyrido<1,2-e>purin-2,4(1H,3H)-dion (79246-61-0) + 3-phenyl-propenal (104-55-2)

Guidance literature:

In dichloromethane; for 72h; Mechanism; Irradiation;

Reference yield:

<5aR-(5aα,6β,9β,10α)>-5,5a,6,9-Tetrahydro-1,3,5-trimethyl-6,9-diphenylpyrido<1,2-e>purin-2,4(1H,3H)-dion (79246-61-0) → 3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione (58-08-2,138455-22-8,95789-13-2) + trans,trans-1,4-Diphenyl-1,3-butadiene (886-65-7,538-81-8)

Guidance literature:

In acetonitrile; at 20 ℃; Irradiation; in dependence on temperature, λ or thermolysis;

upstream raw materials:

3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione

trans,trans-1,4-Diphenyl-1,3-butadiene

Downstream raw materials:

3,7-dihydro-1,3,7-trimethyl-1H-purine-2,6-dione

trans,trans-1,4-Diphenyl-1,3-butadiene

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