Cbz-Ala-ψ[CH2SO2]-Cl

Base Information

Chemical Name:Cbz-Ala-ψ[CH2SO2]-Cl
CAS No.:1140948-95-3
Molecular Formula:C₁₁H₁₄ClNO₄S
Molecular Weight:291.755
Hs Code.:

Synonyms:Cbz-Ala-ψ[CH2SO2]-Cl

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Chemical Property of Cbz-Ala-ψ[CH2SO2]-Cl

Chemical Property:

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Technology Process of Cbz-Ala-ψ[CH2SO2]-Cl

There total 10 articles about Cbz-Ala-ψ[CH2SO2]-Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1300689-92-2
C₁₁H₁₄NO₅S^(1-)*Na⁽¹⁺⁾

: 1140948-95-3
Cbz-Ala-ψ[CH2SO2]-Cl

Guidance literature:: With phosgene; at 20 ℃;
DOI:10.1016/j.tetlet.2009.02.130

Reference yield:

: 1140948-93-1
(S)-2-benzyloxycarbonylaminopropyl thiolacetate

: 1140948-95-3
Cbz-Ala-ψ[CH2SO2]-Cl

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; dihydrogen peroxide; acetic acid / 20 °C

2.1: 10% palladium on activated charcoal; sodium acetate / water / 20 °C

2.2: 20 °C

With 10% palladium on activated charcoal; water; dihydrogen peroxide; sodium acetate; acetic acid; In water;
DOI:10.1016/j.bmc.2011.02.014

Reference yield:

: 6429-44-3,61425-27-2,87905-97-3,66674-16-6
(S)-(-)-N-(benzyloxycarbonyl)alaninol

: 1140948-95-3
Cbz-Ala-ψ[CH2SO2]-Cl

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 0 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

3.1: water; dihydrogen peroxide; acetic acid / 20 °C

4.1: 10% palladium on activated charcoal; sodium acetate / water / 20 °C

4.2: 20 °C

With 10% palladium on activated charcoal; water; dihydrogen peroxide; sodium acetate; caesium carbonate; acetic acid; triethylamine; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.02.014