2'-O-(1,1-dioxo-1λ6-thiomorpholine-4-carbothioate)-N6-benzoyl-adenosine

Base Information

Chemical Name:2'-O-(1,1-dioxo-1λ6-thiomorpholine-4-carbothioate)-N6-benzoyl-adenosine
CAS No.:1219089-97-0
Molecular Formula:C₂₂H₂₄N₆O₇S₂
Molecular Weight:548.601
Hs Code.:

Synonyms:2'-O-(1,1-dioxo-1λ6-thiomorpholine-4-carbothioate)-N6-benzoyl-adenosine

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Chemical Property of 2'-O-(1,1-dioxo-1λ6-thiomorpholine-4-carbothioate)-N6-benzoyl-adenosine

Chemical Property:

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Technology Process of 2'-O-(1,1-dioxo-1λ6-thiomorpholine-4-carbothioate)-N6-benzoyl-adenosine

There total 3 articles about 2'-O-(1,1-dioxo-1λ6-thiomorpholine-4-carbothioate)-N6-benzoyl-adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1219089-96-9
MrA(Bz)DTCT

: 1219089-97-0
2'-O-(1,1-dioxo-1λ6-thiomorpholine-4-carbothioate)-N6-benzoyl-adenosine

Guidance literature:: With pyridine; pyridine hydrogenfluoride; In dichloromethane; acetonitrile;

Reference yield:

: 1219089-95-8
MrA(Bz)TCI

: 1219089-97-0
2'-O-(1,1-dioxo-1λ6-thiomorpholine-4-carbothioate)-N6-benzoyl-adenosine

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 2 h / 20 °C

2: pyridine; hydrogen fluoride / dichloromethane; acetonitrile / 2 h / 0 - 20 °C

With pyridine; hydrogen fluoride; In dichloromethane; acetonitrile;
DOI:10.1021/ja201561z

Reference yield:

: 79154-57-7
3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-N₆-benzoyladenosine

: 1219089-97-0
2'-O-(1,1-dioxo-1λ6-thiomorpholine-4-carbothioate)-N6-benzoyl-adenosine

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / acetonitrile / 3.5 h / 20 °C

2: dichloromethane / 2 h / 20 °C

3: pyridine; hydrogen fluoride / dichloromethane; acetonitrile / 2 h / 0 - 20 °C

With pyridine; dmap; hydrogen fluoride; In dichloromethane; acetonitrile;
DOI:10.1021/ja201561z