(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[(4-methoxyphenyl)carbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-methoxybenzoate

Base Information

Chemical Name:(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[(4-methoxyphenyl)carbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-methoxybenzoate
CAS No.:1559057-72-5
Molecular Formula:C₄₁H₄₆F₂O₉
Molecular Weight:720.808
Hs Code.:

(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[(4-methoxyphenyl)carbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-methoxybenzoate

Synonyms:(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[(4-methoxyphenyl)carbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-methoxybenzoate

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Chemical Property of (1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[(4-methoxyphenyl)carbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-methoxybenzoate

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Technology Process of (1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[(4-methoxyphenyl)carbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-methoxybenzoate

There total 4 articles about (1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[(4-methoxyphenyl)carbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1559057-58-7
(1S,2R,3R,4R)-4-[(4-methoxyphenyl)carbonyloxy]-3-[(1E)-3-oxo-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-methoxybenzoate

: 1559057-72-5
(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[(4-methoxyphenyl)carbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-methoxybenzoate

Guidance literature:: With pyridine hydrogenfluoride; In toluene; at 25 ℃; for 6h;

Reference yield:

: 1559057-77-0,130209-78-8
C₂₅H₃₆O₆

: 1559057-72-5
(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[(4-methoxyphenyl)carbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-methoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; 1,4-dioxane / 11 h / 25 - 40 °C

2: pyridine / dichloromethane / 24 h / 5 - 25 °C

3: pyridine hydrogenfluoride / toluene / 6 h / 25 °C

With pyridine; pyridine hydrogenfluoride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; dichloromethane; toluene;

Reference yield:

: 1559057-74-7
(Z)-isopropyl 7-((1R,5S,6R,7R)-7-((E)-3-hydroxy-4-phenoxybut-1-en-1-yl)-3-phenyl-2,4-dioxa-3-borabicyclo[3.2.1]octan-6-yl)hept-5-enoate

: 1559057-72-5
(1S,2R,3R,4R)-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-4-[(4-methoxyphenyl)carbonyloxy]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-methoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: PCC on alumina / dichloromethane / 3 h / 25 °C

2: pyridine / dichloromethane / 24 h / 5 - 25 °C

3: pyridine hydrogenfluoride / toluene / 6 h / 25 °C

With pyridine; PCC on alumina; pyridine hydrogenfluoride; In dichloromethane; toluene;