C₂₄H₂₃NOSe

Base Information

Chemical Name:C₂₄H₂₃NOSe
CAS No.:939437-97-5
Molecular Formula:C₂₄H₂₃NOSe
Molecular Weight:420.413
Hs Code.:

Synonyms:C₂₄H₂₃NOSe

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Chemical Property of C₂₄H₂₃NOSe

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Technology Process of C₂₄H₂₃NOSe

There total 15 articles about C₂₄H₂₃NOSe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 5707-04-0
Phenylselenyl chloride

: 125287-18-5
glucomaurrol

: 939437-97-5
C₂₄H₂₃NOSe

Guidance literature:: In dichloromethane; at -40 ℃; for 0.75h;
DOI:10.1021/ol070381m

Reference yield:

: 939437-86-2
C₃₁H₄₃NO₄SSi

: 939437-97-5
C₂₄H₂₃NOSe

Guidance literature:: Multi-step reaction with 7 steps

1.1: NaBH₄ / methanol; tetrahydrofuran / 1 h / 0 °C

2.1: Mg; NH₄Cl / methanol; tetrahydrofuran / 5.5 h

3.1: 876 mg / NEt₃ / Pd/C / 1,3,5-trimethyl-benzene / 14 h / Heating

4.1: 82 percent / IBX / ethyl acetate / 1.25 h / Heating

5.1: n-BuLi / tetrahydrofuran; hexane / 0.25 h / 0 °C

5.2: tetrahydrofuran; hexane / 1.25 h

6.1: 125 mg / TBAF / tetrahydrofuran / 0.17 h

7.1: 82 percent / CH₂Cl₂ / 0.75 h / -40 °C

With sodium tetrahydroborate; n-butyllithium; tetrabutyl ammonium fluoride; ammonium chloride; magnesium; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; dichloromethane; ethyl acetate; 1,3,5-trimethyl-benzene; 5.2: Wittig reaction;
DOI:10.1021/ol070381m

Reference yield:

: 939437-93-1
C₃₁H₄₅NO₄SSi

: 939437-97-5
C₂₄H₂₃NOSe

Guidance literature:: Multi-step reaction with 6 steps

1.1: Mg; NH₄Cl / methanol; tetrahydrofuran / 5.5 h

2.1: 876 mg / NEt₃ / Pd/C / 1,3,5-trimethyl-benzene / 14 h / Heating

3.1: 82 percent / IBX / ethyl acetate / 1.25 h / Heating

4.1: n-BuLi / tetrahydrofuran; hexane / 0.25 h / 0 °C

4.2: tetrahydrofuran; hexane / 1.25 h

5.1: 125 mg / TBAF / tetrahydrofuran / 0.17 h

6.1: 82 percent / CH₂Cl₂ / 0.75 h / -40 °C

With n-butyllithium; tetrabutyl ammonium fluoride; ammonium chloride; magnesium; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; dichloromethane; ethyl acetate; 1,3,5-trimethyl-benzene; 4.2: Wittig reaction;
DOI:10.1021/ol070381m