N-(5,5-dimethyl-2-phenylamino-4H-imidazol-4-on-3-yl)iminotriphenylphosphorane

Base Information

Chemical Name:N-(5,5-dimethyl-2-phenylamino-4H-imidazol-4-on-3-yl)iminotriphenylphosphorane
CAS No.:915068-38-1
Molecular Formula:C₂₉H₂₇N₄OP
Molecular Weight:478.533
Hs Code.:

Synonyms:N-(5,5-dimethyl-2-phenylamino-4H-imidazol-4-on-3-yl)iminotriphenylphosphorane

Suppliers and Price of N-(5,5-dimethyl-2-phenylamino-4H-imidazol-4-on-3-yl)iminotriphenylphosphorane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(5,5-dimethyl-2-phenylamino-4H-imidazol-4-on-3-yl)iminotriphenylphosphorane

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Technology Process of N-(5,5-dimethyl-2-phenylamino-4H-imidazol-4-on-3-yl)iminotriphenylphosphorane

There total 2 articles about N-(5,5-dimethyl-2-phenylamino-4H-imidazol-4-on-3-yl)iminotriphenylphosphorane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 915068-37-0
3-amino-5,5-dimethyl-2-phenylamino-4H-imidazol-4-one

: 603-35-0
triphenylphosphine

: 915068-38-1
N-(5,5-dimethyl-2-phenylamino-4H-imidazol-4-on-3-yl)iminotriphenylphosphorane

Guidance literature:: With hexachloroethane; triethylamine; In acetonitrile; at 20 ℃; for 5h;
DOI:10.1002/ejoc.200600201

Reference yield:

: 915068-35-8
N-(1-ethoxycarbonyl-1-methylethyl)-N'-phenylcarbodiimide

: 915068-38-1
N-(5,5-dimethyl-2-phenylamino-4H-imidazol-4-on-3-yl)iminotriphenylphosphorane

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / hydrazine hydrate / acetonitrile / 1 h / 20 °C

2: 83 percent / hexachloroethane; triethylamine / acetonitrile / 5 h / 20 °C

With hexachloroethane; hydrazine hydrate; triethylamine; In acetonitrile;
DOI:10.1002/ejoc.200600201