4-(3-((2-(benzyloxy)-4-chlorophenoxy)methyl)phenyl)-4-methoxytetrahydro-2H-pyran

Base Information

Chemical Name:4-(3-((2-(benzyloxy)-4-chlorophenoxy)methyl)phenyl)-4-methoxytetrahydro-2H-pyran
CAS No.:1289486-13-0
Molecular Formula:C₂₆H₂₇ClO₄
Molecular Weight:438.951
Hs Code.:

Synonyms:4-(3-((2-(benzyloxy)-4-chlorophenoxy)methyl)phenyl)-4-methoxytetrahydro-2H-pyran

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Chemical Property of 4-(3-((2-(benzyloxy)-4-chlorophenoxy)methyl)phenyl)-4-methoxytetrahydro-2H-pyran

Chemical Property:

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Technology Process of 4-(3-((2-(benzyloxy)-4-chlorophenoxy)methyl)phenyl)-4-methoxytetrahydro-2H-pyran

There total 8 articles about 4-(3-((2-(benzyloxy)-4-chlorophenoxy)methyl)phenyl)-4-methoxytetrahydro-2H-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 381220-85-5
2-(benzyloxy)-4-chlorophenol

: 144800-91-9
4-(3-(bromomethyl)phenyl)-4-methoxytetrahydro-2H-pyran

: 1289486-13-0
4-(3-((2-(benzyloxy)-4-chlorophenoxy)methyl)phenyl)-4-methoxytetrahydro-2H-pyran

Guidance literature:: With potassium carbonate; In acetone; Reflux;
DOI:10.1016/j.bmc.2011.01.043

Reference yield:

: 29943-42-8,143562-54-3
Tetrahydro-4H-pyran-4-one

: 1289486-13-0
4-(3-((2-(benzyloxy)-4-chlorophenoxy)methyl)phenyl)-4-methoxytetrahydro-2H-pyran

Guidance literature:: Multi-step reaction with 4 steps

1.1: magnesium / tetrahydrofuran / Reflux

1.2: 1 h / Reflux

2.1: sodium hydride / tetrahydrofuran; mineral oil / 15 h / 20 °C

3.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 1.5 h / Reflux

4.1: potassium carbonate / acetone / Reflux

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydride; potassium carbonate; magnesium; In tetrahydrofuran; tetrachloromethane; acetone; mineral oil;
DOI:10.1016/j.bmc.2011.01.043

Reference yield:

: 6272-38-4
O-benzylcatechol

: 1289486-13-0
4-(3-((2-(benzyloxy)-4-chlorophenoxy)methyl)phenyl)-4-methoxytetrahydro-2H-pyran

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuryl dichloride / toluene / 1 h / 20 °C

2: potassium carbonate / acetone / Reflux

With sulfuryl dichloride; potassium carbonate; In acetone; toluene;
DOI:10.1016/j.bmc.2011.01.043