(1R,4S)-4-Ethyl-4-(2-hydroxy-ethyl)-cyclohex-2-enol

Base Information

Chemical Name:(1R,4S)-4-Ethyl-4-(2-hydroxy-ethyl)-cyclohex-2-enol
CAS No.:403511-47-7
Molecular Formula:C₁₀H₁₈O₂
Molecular Weight:170.252
Hs Code.:

Synonyms:(1R,4S)-4-Ethyl-4-(2-hydroxy-ethyl)-cyclohex-2-enol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,4S)-4-Ethyl-4-(2-hydroxy-ethyl)-cyclohex-2-enol

Chemical Property:

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Technology Process of (1R,4S)-4-Ethyl-4-(2-hydroxy-ethyl)-cyclohex-2-enol

There total 8 articles about (1R,4S)-4-Ethyl-4-(2-hydroxy-ethyl)-cyclohex-2-enol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 403511-46-6
2-[(1S,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-1-ethyl-cyclohex-2-enyl]-ethanol

: 403511-47-7
(1R,4S)-4-Ethyl-4-(2-hydroxy-ethyl)-cyclohex-2-enol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(01)02075-5

Reference yield:

: 403511-40-0
C₁₃H₁₇BrO₂

: 403511-47-7
(1R,4S)-4-Ethyl-4-(2-hydroxy-ethyl)-cyclohex-2-enol

Guidance literature:: Multi-step reaction with 7 steps

1: 96 percent / diphenyl ether / 280 °C

2: 92 percent / H₂ / Pd/C / ethyl acetate

3: 93 percent / Zn / acetic acid; methanol / Heating

4: 94 percent / imidazole / 20 °C

5: 93 percent / NaHCO₃ / diphenyl ether / 280 °C

6: 84 percent / LiEt₃BH / tetrahydrofuran / 20 °C

7: 99 percent / TBAF / tetrahydrofuran

With 1H-imidazole; tetrabutyl ammonium fluoride; hydrogen; lithium triethylborohydride; sodium hydrogencarbonate; zinc; palladium on activated charcoal; In tetrahydrofuran; methanol; diphenylether; acetic acid; ethyl acetate;
DOI:10.1016/S0040-4039(01)02075-5

Reference yield:

: C₁₅H₁₉BrO₃

: 403511-47-7
(1R,4S)-4-Ethyl-4-(2-hydroxy-ethyl)-cyclohex-2-enol

Guidance literature:: Multi-step reaction with 8 steps

1: 98 percent / K₂CO₃; MeOH / 20 °C

2: 96 percent / diphenyl ether / 280 °C

3: 92 percent / H₂ / Pd/C / ethyl acetate

4: 93 percent / Zn / acetic acid; methanol / Heating

5: 94 percent / imidazole / 20 °C

6: 93 percent / NaHCO₃ / diphenyl ether / 280 °C

7: 84 percent / LiEt₃BH / tetrahydrofuran / 20 °C

8: 99 percent / TBAF / tetrahydrofuran

With 1H-imidazole; methanol; tetrabutyl ammonium fluoride; hydrogen; lithium triethylborohydride; sodium hydrogencarbonate; potassium carbonate; zinc; palladium on activated charcoal; In tetrahydrofuran; methanol; diphenylether; acetic acid; ethyl acetate;
DOI:10.1016/S0040-4039(01)02075-5