2-[(1S,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-1-ethyl-cyclohex-2-enyl]-ethanol

Base Information

Chemical Name:2-[(1S,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-1-ethyl-cyclohex-2-enyl]-ethanol
CAS No.:403511-46-6
Molecular Formula:C₁₆H₃₂O₂Si
Molecular Weight:284.514
Hs Code.:

Synonyms:2-[(1S,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-1-ethyl-cyclohex-2-enyl]-ethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(1S,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-1-ethyl-cyclohex-2-enyl]-ethanol

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Technology Process of 2-[(1S,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-1-ethyl-cyclohex-2-enyl]-ethanol

There total 7 articles about 2-[(1S,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-1-ethyl-cyclohex-2-enyl]-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 403511-45-5
2-[4-(tert-butyl-dimethyl-silanyloxy)-1-ethyl-cyclohex-2-enyl]-N,N-dimethyl-acetamide

: 403511-46-6
2-[(1S,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-1-ethyl-cyclohex-2-enyl]-ethanol

Guidance literature:: With lithium triethylborohydride; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/S0040-4039(01)02075-5

Reference yield:

: 403511-40-0
C₁₃H₁₇BrO₂

: 403511-46-6
2-[(1S,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-1-ethyl-cyclohex-2-enyl]-ethanol

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / diphenyl ether / 280 °C

2: 92 percent / H₂ / Pd/C / ethyl acetate

3: 93 percent / Zn / acetic acid; methanol / Heating

4: 94 percent / imidazole / 20 °C

5: 93 percent / NaHCO₃ / diphenyl ether / 280 °C

6: 84 percent / LiEt₃BH / tetrahydrofuran / 20 °C

With 1H-imidazole; hydrogen; lithium triethylborohydride; sodium hydrogencarbonate; zinc; palladium on activated charcoal; In tetrahydrofuran; methanol; diphenylether; acetic acid; ethyl acetate;
DOI:10.1016/S0040-4039(01)02075-5

Reference yield:

: C₁₅H₁₉BrO₃

: 403511-46-6
2-[(1S,4R)-4-(tert-Butyl-dimethyl-silanyloxy)-1-ethyl-cyclohex-2-enyl]-ethanol

Guidance literature:: Multi-step reaction with 7 steps

1: 98 percent / K₂CO₃; MeOH / 20 °C

2: 96 percent / diphenyl ether / 280 °C

3: 92 percent / H₂ / Pd/C / ethyl acetate

4: 93 percent / Zn / acetic acid; methanol / Heating

5: 94 percent / imidazole / 20 °C

6: 93 percent / NaHCO₃ / diphenyl ether / 280 °C

7: 84 percent / LiEt₃BH / tetrahydrofuran / 20 °C

With 1H-imidazole; methanol; hydrogen; lithium triethylborohydride; sodium hydrogencarbonate; potassium carbonate; zinc; palladium on activated charcoal; In tetrahydrofuran; methanol; diphenylether; acetic acid; ethyl acetate;
DOI:10.1016/S0040-4039(01)02075-5