(+)-(S)-N-[(1R,2S)-2-benzylamino-3-(tert-butyldiphenylsilyloxy)-1-(iso-propyl)prop-1-yl]-p-tolylsulfinamide

Base Information

Chemical Name:(+)-(S)-N-[(1R,2S)-2-benzylamino-3-(tert-butyldiphenylsilyloxy)-1-(iso-propyl)prop-1-yl]-p-tolylsulfinamide
CAS No.:1099822-32-8
Molecular Formula:C₃₆H₄₆N₂O₂SSi
Molecular Weight:598.925
Hs Code.:

Synonyms:(+)-(S)-N-[(1R,2S)-2-benzylamino-3-(tert-butyldiphenylsilyloxy)-1-(iso-propyl)prop-1-yl]-p-tolylsulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(S)-N-[(1R,2S)-2-benzylamino-3-(tert-butyldiphenylsilyloxy)-1-(iso-propyl)prop-1-yl]-p-tolylsulfinamide

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Technology Process of (+)-(S)-N-[(1R,2S)-2-benzylamino-3-(tert-butyldiphenylsilyloxy)-1-(iso-propyl)prop-1-yl]-p-tolylsulfinamide

There total 1 articles about (+)-(S)-N-[(1R,2S)-2-benzylamino-3-(tert-butyldiphenylsilyloxy)-1-(iso-propyl)prop-1-yl]-p-tolylsulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 467471-31-4
(+)-(2S,3R,S_S)-2-(benzylamino)-4-methyl-3-(p-tolylsulfinylamino)pentan-1-ol

: 1099822-32-8
(+)-(S)-N-[(1R,2S)-2-benzylamino-3-(tert-butyldiphenylsilyloxy)-1-(iso-propyl)prop-1-yl]-p-tolylsulfinamide

Guidance literature:: With 1H-imidazole; dmap; In dichloromethane; at 20 ℃; for 5.5h; Inert atmosphere;
DOI:10.1016/j.tet.2008.10.034

Reference yield: 85.0%

: 1099822-32-8
(+)-(S)-N-[(1R,2S)-2-benzylamino-3-(tert-butyldiphenylsilyloxy)-1-(iso-propyl)prop-1-yl]-p-tolylsulfinamide

: 79-04-9
chloroacetyl chloride

: 1099822-33-9
(+)-N-benzyl-N-[(1S,2R)-1-(tert-butyldiphenylsilyloxymethyl)-3-methyl-2-((S)-p-tolylsulfinylamino)but-1-yl]-2-chloroacetamide

Guidance literature:: With sodium hydrogencarbonate; In water; ethyl acetate; at 0 - 20 ℃; for 2.5h; Inert atmosphere; Saturated solution;
DOI:10.1016/j.tet.2008.10.034