1-hydroxy-4-methyl-cyclohexanecarboxylic acid-(4-methyl-cyclohex-1-enyl ester)

Base Information

• Chemical Name: 1-hydroxy-4-methyl-cyclohexanecarboxylic acid-(4-methyl-cyclohex-1-enyl ester)
• CAS No.: 94092-43-0
• Molecular Formula: C₁₅H₂₄O₃
• Molecular Weight: 252.354

Synonyms:1-hydroxy-4-methyl-cyclohexanecarboxylic acid-(4-methyl-cyclohex-1-enyl ester)

Chemical Property of 1-hydroxy-4-methyl-cyclohexanecarboxylic acid-(4-methyl-cyclohex-1-enyl ester)

Chemical Property:

Purity/Quality:

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Technology Process of 1-hydroxy-4-methyl-cyclohexanecarboxylic acid-(4-methyl-cyclohex-1-enyl ester)

There total 2 articles about 1-hydroxy-4-methyl-cyclohexanecarboxylic acid-(4-methyl-cyclohex-1-enyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

potassium cyanide (151-50-8) + 1-methylcyclohexan-4-one (589-92-4) → 1-hydroxy-4-methyl-cyclohexanecarboxylic acid-(4-methyl-cyclohex-1-enyl ester) (94092-43-0)

Guidance literature:

With sodium hydrogensulfite; Erhitzen des Reaktionsgemisches mit wss. Salzsaeure;

DOI:10.1007/PL00009877

Reference yield:

→ 1-hydroxy-4-methyl-cyclohexanecarboxylic acid-(4-methyl-cyclohex-1-enyl ester) (94092-43-0)

Guidance literature:

1-Cyan-4-methyl-cyclohexanol, konz. HCl, (neben 1-Hydroxy-4-methyl-cyclohexancarbonsaeure);

DOI:10.1039/jr9640001413

Reference yield:

1-hydroxy-4-methyl-cyclohexanecarboxylic acid-(4-methyl-cyclohex-1-enyl ester) (94092-43-0) → 1-hydroxy-4-methyl-cyclohexanecarboxylic acid (41248-15-1) + 1-methylcyclohexan-4-one (589-92-4)

Guidance literature:

With potassium hydroxide; substance of mp: 82 degree;

DOI:10.1007/PL00009877 DOI:10.1039/jr9640001413

upstream raw materials:

potassium cyanide

1-methylcyclohexan-4-one

Downstream raw materials:

1-hydroxy-4-methyl-cyclohexanecarboxylic acid

1-methylcyclohexan-4-one

1-hydroxy-4-methyl-cyclohexanecarbonitrile

1-hydroxy-4-methyl-cyclohexanecarboxylic acid methyl ester

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