2',3'-O-isopropylidene-5'-O-(di-tert-butylphosphoramidite)-6-(2,4-dinitrophenyl)thioinosine

Base Information

Chemical Name:2',3'-O-isopropylidene-5'-O-(di-tert-butylphosphoramidite)-6-(2,4-dinitrophenyl)thioinosine
CAS No.:1359697-42-9
Molecular Formula:C₂₇H₃₇N₆O₁₁PS
Molecular Weight:684.664
Hs Code.:

Synonyms:2',3'-O-isopropylidene-5'-O-(di-tert-butylphosphoramidite)-6-(2,4-dinitrophenyl)thioinosine

Suppliers and Price of 2',3'-O-isopropylidene-5'-O-(di-tert-butylphosphoramidite)-6-(2,4-dinitrophenyl)thioinosine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2',3'-O-isopropylidene-5'-O-(di-tert-butylphosphoramidite)-6-(2,4-dinitrophenyl)thioinosine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2',3'-O-isopropylidene-5'-O-(di-tert-butylphosphoramidite)-6-(2,4-dinitrophenyl)thioinosine

There total 5 articles about 2',3'-O-isopropylidene-5'-O-(di-tert-butylphosphoramidite)-6-(2,4-dinitrophenyl)thioinosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₃₇N₆O₁₀PS

: 1359697-42-9
2',3'-O-isopropylidene-5'-O-(di-tert-butylphosphoramidite)-6-(2,4-dinitrophenyl)thioinosine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 ℃;
DOI:10.1021/jm201127y

Reference yield:

: 60095-36-5,5856-48-4
2',3'-O-isopropylidene-6-thioinosine

: 1359697-42-9
2',3'-O-isopropylidene-5'-O-(di-tert-butylphosphoramidite)-6-(2,4-dinitrophenyl)thioinosine

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / acetonitrile / 1 h / 20 °C

2: 1H-tetrazole / dichloromethane / 1 h / 20 °C

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -78 °C

With 1H-tetrazole; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile;
DOI:10.1021/jm201127y

Reference yield:

: 1359697-38-3
2',3'-O-isopropylidene-6-(2,4-dinitrophenyl)thioinosine

: 1359697-42-9
2',3'-O-isopropylidene-5'-O-(di-tert-butylphosphoramidite)-6-(2,4-dinitrophenyl)thioinosine

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-tetrazole / dichloromethane / 1 h / 20 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -78 °C

With 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jm201127y