(S)-2-(3-hydroxy-1-methylpropyl)phenol

Base Information

Chemical Name:(S)-2-(3-hydroxy-1-methylpropyl)phenol
CAS No.:164265-05-8
Molecular Formula:C₁₀H₁₄O₂
Molecular Weight:166.22
Hs Code.:

Synonyms:(S)-2-(3-hydroxy-1-methylpropyl)phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-(3-hydroxy-1-methylpropyl)phenol

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Technology Process of (S)-2-(3-hydroxy-1-methylpropyl)phenol

There total 5 articles about (S)-2-(3-hydroxy-1-methylpropyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 30825-54-8
(S)-3,4-dihydro-4-methylcoumarin

: 164265-05-8
(S)-2-(3-hydroxy-1-methylpropyl)phenol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1016/0957-4166(95)00111-2

Reference yield: 3.8%

: (R)-3-(4-dimethylamino-2-methoxyphenyl)-butanol tert-butyldimethylsilyl ether

: 164265-05-8
(S)-2-(3-hydroxy-1-methylpropyl)phenol

Guidance literature:: (R)-3-(4-dimethylamino-2-methoxyphenyl)-butanol tert-butyldimethylsilyl ether; With methyl iodide; In diethyl ether; for 10h;

With methanol; hydrogen bromide; sodium; In diethyl ether; ammonia; at -78 - 20 ℃; for 8.05h;

Reference yield:

: 68679-84-5
(S)-3-phenyl butyric acid chloride

: 164265-05-8
(S)-2-(3-hydroxy-1-methylpropyl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / dichloromethane / 1 h / 0 °C / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid / dichloromethane / 14 h / 60 °C / Inert atmosphere

3: lithium aluminium tetrahydride / tetrahydrofuran / 0.75 h / 0 °C / Inert atmosphere

With aluminum (III) chloride; lithium aluminium tetrahydride; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja110052n