2,3-dihydroxypropyl 11-{[(2E)-3-(4-hydroxy-3-methoxyphenyl)prop-2-enoyl]oxy}undecanoate

Base Information

Chemical Name:2,3-dihydroxypropyl 11-{[(2E)-3-(4-hydroxy-3-methoxyphenyl)prop-2-enoyl]oxy}undecanoate
CAS No.:1428651-36-8
Molecular Formula:C₂₄H₃₆O₈
Molecular Weight:452.545
Hs Code.:

Synonyms:2,3-dihydroxypropyl 11-{[(2E)-3-(4-hydroxy-3-methoxyphenyl)prop-2-enoyl]oxy}undecanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-dihydroxypropyl 11-{[(2E)-3-(4-hydroxy-3-methoxyphenyl)prop-2-enoyl]oxy}undecanoate

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Technology Process of 2,3-dihydroxypropyl 11-{[(2E)-3-(4-hydroxy-3-methoxyphenyl)prop-2-enoyl]oxy}undecanoate

There total 5 articles about 2,3-dihydroxypropyl 11-{[(2E)-3-(4-hydroxy-3-methoxyphenyl)prop-2-enoyl]oxy}undecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: (E)-(2, 2-dimethyl-1,3-dioxolan-4-yl)methyl 11-(3-(4-hydroxy-3-methoxyphenyl)acryloyloxy)undecanoate

: 1428651-36-8
2,3-dihydroxypropyl 11-{[(2E)-3-(4-hydroxy-3-methoxyphenyl)prop-2-enoyl]oxy}undecanoate

Guidance literature:: With hydrogenchloride; water; In methanol; at 20 ℃; for 4h; Cooling with ice;
DOI:10.1016/j.btre.2019.e00375

Reference yield:

: 2834-05-1
11-bromoundecanoic acid

: 1428651-36-8
2,3-dihydroxypropyl 11-{[(2E)-3-(4-hydroxy-3-methoxyphenyl)prop-2-enoyl]oxy}undecanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / water / 16 h / 100 °C

1.2: 25 °C / pH 1

2.1: immobilized lipase from Candida antarctica / hexane; butanone / 60 °C / Enzymatic reaction

3.1: immobilized lipase from Candida antarctica / hexane; butanone / 60 °C / Enzymatic reaction

4.1: water; hydrogenchloride / methanol / 4 h / 20 °C / Cooling with ice

With hydrogenchloride; water; potassium hydroxide; In methanol; hexane; water; butanone;
DOI:10.1016/j.btre.2019.e00375

Reference yield:

: 1135-24-6,537-98-4
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid

: 1428651-36-8
2,3-dihydroxypropyl 11-{[(2E)-3-(4-hydroxy-3-methoxyphenyl)prop-2-enoyl]oxy}undecanoate

Guidance literature:: Multi-step reaction with 4 steps

1: mercury(II) diacetate; sulfuric acid / tetrahydrofuran / 12 h / 40 °C / Inert atmosphere

2: immobilized lipase from Candida antarctica / hexane; butanone / 60 °C / Enzymatic reaction

3: immobilized lipase from Candida antarctica / hexane; butanone / 60 °C / Enzymatic reaction

4: water; hydrogenchloride / methanol / 4 h / 20 °C / Cooling with ice

With hydrogenchloride; sulfuric acid; mercury(II) diacetate; water; In tetrahydrofuran; methanol; hexane; butanone;
DOI:10.1016/j.btre.2019.e00375